Abstract-We demonstrate a new digital etch technique for controllably thinning III-V semiconductor heterostructures with sub-1-nm resolution. This is a two-step process consisting of lowpower O 2 plasma oxidation, followed by diluted H 2 SO 4 rinse for selective oxide removal. This approach can etch a combination of InP, InGaAs, and InAlAs in a precise and nonselective manner. We have also developed a method to determine the etch rate per cycle, and to control the etch depth in actual device structures. For InP, the etch rate is ∼0.9 nm/cycle. We illustrate the new process by fabricating L g = 60-nm selfaligned buried-channel InGaAs MOSFETs. These devices feature a composite gate dielectric consisting of 1-nm InP and 2-nm HfO 2 for an overall sub-1-nm effective oxide thickness. A typical device shows a peak transconductance of 1.53 mS/µm (V ds = 0.5 V), subthreshold swing of 89 mV/decade, and 102 mV/decade at V ds = 0.05 and 0.5 V, respectively, and ON current of 326 µA/µm at I OFF = 100 nA/µm and V dd = 0.5 V.