A brief review of established methods shows that only with the Berthelot technique is it possible to see a finite volume of liquid in sustained mechanical tension. A short discussion of the practice and theory reveals two uncertainties with the conventional technique : that of the determination of a true filling temperature, and the influence of compliance by the glass on the tension developed. A description is then given of a modified apparatus with which these difficulties do not arise. The tube is formed into a coil which deflects sufficiently to indicate internal pressure or tension, and by monitoring these deflections with a distance meter a record of pressure/ tension against temperature can be made. The course of a typical run is shown from which the excess pressure, filling temperature and limiting tension may all be estimated with much greater precision than befoie. The orders of magnitude of the results obtained are indicated, and a possible influence of non-uniform gaseous supersaturation is suggested.
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Articles you may be interested inMechanism maps for electromigration-induced failure of metal and alloy interconnects Theoretical analysis of electromigration-induced failure of metallic thin films due to transgranular void propagation Electromigration-induced failures in high-temperature sputtered Al-alloy metallization have been studied in terms of Al-alloy microstructure, Si nodules, and reaction products between the Al alloy and the underlayer material. Highly reliable interconnects can be realized by high-temperature sputtered Al-Si-Cu-alloy metallization utilizing a Ti underlayer. The interfacial reaction between the growing Al-Si-Cu film and the Ti underlayer during high-temperature sputtering produces an Al 3 Ti-alloy layer having a resistivity of about 40 ⍀ cm, and Si in Al alloy is absorbed in the Al 3 Ti layer without forming Si nodules. As the result, a bilayer structure of Al alloy/Al-Ti-Si alloy is formed. The electromigration resistance of the resultant TiN/Al alloy/Al-Ti-Si/TiN structure is drastically improved. It is speculated from the experimental results that this is because of the high quality of the Al-alloy film microstructure, i.e., an increase in ͑111͒ orientation, a decrease in the standard deviation of the grain distribution, and the superior current bypass effect through the Al-Ti-Si alloy and underlying TiN layer. In particular, an electrical current easily flows through the Al-Ti-Si alloy and TiN layer before a void completely crosses the upper Al alloy part of the metal line because the formation of the AlN high-resistance layer is suppressed by laying the Ti film between the Al-Si-Cu film and the underlying TiN film. Accordingly, the local temperature increase in the vicinity of the void is not essential to the subsequent void growth due to the lower resistivity of the Al-Ti-Si-alloy layer, resulting in the low void growth rate.
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