Conductive polymer composites are manufactured by randomly dispersing conductive particles along an insulating polymer matrix. Several authors have attempted to model the piezoresistive response of conductive polymer composites. However, all the proposed models rely upon experimental measurements of the electrical resistance at rest state. Similarly, the models available in literature assume a voltage-independent resistance and a stress-independent area for tunneling conduction. With the aim of developing and validating a more comprehensive model, a test bench capable of exerting controlled forces has been developed. Commercially available sensors—which are manufactured from conductive polymer composites—have been tested at different voltages and stresses, and a model has been derived on the basis of equations for the quantum tunneling conduction through thin insulating film layers. The resistance contribution from the contact resistance has been included in the model together with the resistance contribution from the conductive particles. The proposed model embraces a voltage-dependent behavior for the composite resistance, and a stress-dependent behavior for the tunneling conduction area. The proposed model is capable of predicting sensor current based upon information from the sourcing voltage and the applied stress. This study uses a physical (non-phenomenological) approach for all the phenomena discussed here.
Force Sensing Resistors (FSRs) are manufactured by sandwiching a Conductive Polymer Composite (CPC) between metal electrodes. The piezoresistive property of FSRs has been exploited to perform stress and strain measurements, but the rheological property of polymers has undermined the repeatability of measurements causing creep in the electrical resistance of FSRs. With the aim of understanding the creep phenomenon, the drift response of thirty two specimens of FSRs was studied using a statistical approach. Similarly, a theoretical model for the creep response was developed by combining the Burger’s rheological model with the equations for the quantum tunneling conduction through thin insulating films. The proposed model and the experimental observations showed that the sourcing voltage has a strong influence on the creep response; this observation—and the corresponding model—is an important contribution that has not been previously accounted. The phenomenon of sensitivity degradation was also studied. It was found that sensitivity degradation is a voltage-related phenomenon that can be avoided by choosing an appropriate sourcing voltage in the driving circuit. The models and experimental observations from this study are key aspects to enhance the repeatability of measurements and the accuracy of FSRs.
This article upgrades the RC linear model presented for piezoresistive force sensors. Amplitude nonlinearity is found in sensor conductance, and a characteristic equation is formulated for modeling its response under DC-driving voltages below 1 V. The feasibility of such equation is tested on four FlexiForce model A201-100 piezoresistive sensors by varying the sourcing voltage and the applied forces. Since the characteristic equation proves to be valid, a method is presented for obtaining a specific sensitivity in sensor response by calculating the appropriate sourcing voltage and feedback resistor in the driving circuit; this provides plug-and-play capabilities to the device and reduces the start-up time of new applications where piezoresistive devices are to be used. Finally, a method for bypassing the amplitude nonlinearity is presented with the aim of reading sensor capacitance.
Piezoresistive force sensors exhibit considerable lower accuracy compared with load cells and force measuring systems based in strain gauges, however a new method for measuring forces using piezoresistive sensors is described in this paper, leading to a considerable increase in the repeatability of force readings. The new method consists of reading sensor's conductance and capacitance by applying DC and sinusoidal waveforms, thereby allow us to determine a multivariable estimation of force, instead of using the traditional, purely resistive model that has been used up to now. A study of sensor nonlinearities is also described which will allow us to determine the optimal setup to perform capacitance readings under sinusoidal excitation.
Force Sensing Resistors (FSRs) are manufactured from a blend of conductive nanoparticles dispersed in an insulating polymer matrix. FSRs exhibit large amounts of hysteresis and drift error, but currently, a great effort is placed on improving their performance through different techniques applied during sensor manufacturing. In this article, a novel technique for improving the performance of FSRs is presented; the method can be applied to already-manufactured sensors, which is a clear benefit of the proposed procedure. The method is based on driving the sensors with a modified-astable 555 oscillator, in which the oscillation frequency is set from the sensor's capacitance and resistance. Considering that the sensor's capacitance and resistance have opposite signs in the drift characteristic, the driving circuit provides self-compensated force measurements over extended periods of time. The feasibility of the driving circuit to reduce hysteresis and to avoid sensitivity degradation is also tested. In order to obtain representative results, the experimental measurements from this study were performed over eight FlexiForce A201-25 sensors.
The coating of polymeric substrate polyetheretherketone (PEEK) with silver nanoparticles (AgNPs) was carried out by a wet chemical route at room temperature. The coating process was developed from the Tollens reagent and D-glucose as reducing agent. The resulting composite exhibited antimicrobial activity. The PEEK films were coated with a single layer and two layers of silver nanoparticles in various concentrations. The crystallographic properties of the polymer and the silver nanoparticles were analyzed by X-ray diffraction (XRD). Fourier transform infrared spectra (FTIR) show the interaction between the silver nanoparticles with the polymeric substrate. Transmission electron microscope (TEM) images confirmed the obtaining of metallic nanoparticles with average sizes of 25 nm. It was possible to estimate the amount of silver deposited on PEEK with the help of thermogravimetric analysis. The morphology and shape of the AgNPs uniformly deposited on the PEEK films was ascertained by the techniques of scanning electron microscopy (SEM) and atomic force microscopy (AFM), evidencing the increase in the amount of silver by increasing the concentration of the metal precursor. Finally, the antibacterial activity of the films coated with Ag in Escherichia coli, Serratia marcescens and Bacillus licheniformis was evaluated, evidencing that the concentration of silver is crucial in the cellular replication of the bacteria.
Force-sensing resistors (FSRs) are inexpensive alternatives to load cells. They are suitable for applications where noninvasive devices are needed to measure force, stress, or pressure. However, they have been proved to be hysteresis prone and offer nonrepeatable readings due to their highly voltage-dependent electrical resistance. A piezocapacitive effect has been found as an alternative phenomenon that is able to offer force-dependent readings of capacitance with less hysteresis error. Also, this capacitance is not dependent on voltage, which also improves repeatability in force measurements. Since measuring capacitance is more expensive than resistance, the least costly conditioning circuitry is desired. An inexpensive alternative using an LM555 that oscillates depending on capacitance is here presented. Hysteresis and repeatability errors have been reduced for a widespread-used force-sensing resistor brand.
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