The reaction of silver nitrate with Ph3SbBr 2 in an ethanol-acetone solution afforded the complex [Ph3Sb(NO3)120 9 Me2C=O (I). According to the data of X-ray diffraction study of crystals of I, molecule I contains a nonlinear O-bridge, which links two Sb atoms. The Sb atoms have a trigonal-bipyramidal configuration. The NO 3 group and the bridging oxygen atom are in axial positions and the three Ph substituents are in equatorial positions.
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