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A self-sensitized [2 + 2] cycloaddition process is developed to convert biomass-derived β-pinene and isophorone to high-performance spiro-fuel, which possesses high density and excellent cryogenic properties.

Biofuels synthesized from lignocellulose-derived platform chemicals are very attractive for sustainable development.

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High-energy-density fuels are synthesized through self-photosensitized [2 + 2] cycloaddition of isophorone and a wide range of olefins.