The da r kbrow n co m pou nd [ N ( Me)4]4[As"'8V'V, 4042( 0. 5H20)], co nta i n i ng a sp h e ri ca I a n ion [AsII18VIV1 4042(0. 5H20)]4containing condensed V05 square pyramids and As205 units, is synthesized hydrothermally from As203, V205 and (MeJ4NOH and structurally characterized by X-ray diffraction.
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