The linear (r41) and quadratic (R11 and R12) electro-optic coefficients of GaAs have been measured at the wavelengths 1.32 and 1.52 μm using single-mode AlGaAs/GaAs strip-loaded waveguides. The results are r41=−(1.54±0.08)×10−10 cm/V, R11=−(9.3±2.8)×10−17 cm2/V2 and R12=−(5.1±l.9)×10−17 cm2/V2 at 1.32 μm and r41=−(1.50±0.08)×10−10 cm/V, R11=−(3.2±2.3)×10−17 cm2/V2 and R12=−(5.1±2.6)×10−17 cm2/V2 at 1.52 μm. These results, together with those previously measured at different wavelengths, are compared with published theoretical models. The linear electro-optic coefficient r41 is slightly dispersive near the band gap and roughly constant for longer wavelengths, in good agreement with the models. The quadratic electro-optic coefficients drop rapidly with increasing wavelength, in good agreement with a model based on electroabsorption.
In this paper the simple accelerometers based on PZT thin films were developed and cbaracterized. The functions of seismic mass and spring are given by a boss loaded cantilever structure. The strain of the cantilever is detected by a Pb(Zr,Ti)O, thin film. A 2 mm long and 0.8 mm wide cantilever yielded a response of 0.6 mV/g' in the frequency interval between 1 and 600 Hz. With Af = 600Hz a limit of about lmg* at lHz, and less above this frequency, was observed. The response predicted by the analytical model is close to the actual response of the device. A working miniaturized accelerometer prototype could be thus demonstrated.
Two methods for the determination of iodine in urine or serum based on the Sandell-Kolthoff reaction were compared. The first was an autoanalyser method (AAII, Technicon) where the mineralisation takes place in a continuous flow manner. This procedure was used at the Department of Clinical Chemistry of the University Hospital of Berne (Switzerland) from 1968 until 1993. The second method was evaluated and adapted in our own laboratory. Each sample and the iodate-standards are mineralised in a Pyrex glass tube and the decolorisation reaction takes place in a 96-well-microtiter plate which was read by a PC-controlled photometer at 405 nm. This method, with a detection limit of 0.1 micromol/l showed good analytical recovery (90 to 110%) and a low imprecision (intra-assay coefficient of variation (CV) of 5% and an inter-assay CV of 7.5%). In contrast to the autoanalyser method, the microtiter plate-method is suitable both for series up to 24 samples (3-fold) and for single samples. A comparison of 87 samples in the range of 0.1 to 60 micromol/l which were measured with both Sandell-Kolthoff based methods showed no obvious discrepancy. These two methods showed a good agreement for the determination of urinary iodine. This guarantees that the results of earlier epidemiological studies can be compared with recent studies performed in our and many other laboratories.
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