2013
DOI: 10.1590/s0102-695x2013000600001
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Saponins, tannins and flavonols found in hydroethanolic extract from Periandra dulcis roots

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Cited by 37 publications
(18 citation statements)
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“…49 The fragmentation of the precursor ion at m/z 777 (23) tified as a nortriterpenoid saponin derivative. 24 Similar fragmentation patterns were observed for the precursor ions m/z 909 (22), 747 (29) and 601 (30). 37,40,41 The second-order mass spectra of the precursor ions of m/z 1087 (18), 793 (19), 925 (24), 895 (25) and 631 (26) showed the product ion Y 0 − at m/z 455, which corresponds to the deprotonated aglycone [A−H] − of the oleanolic acid ( Figure 4, Table 1).…”
Section: The Analysis Of the Ms/ms Mass Spectra Of The Precursor Ions Ofsupporting
confidence: 74%
“…49 The fragmentation of the precursor ion at m/z 777 (23) tified as a nortriterpenoid saponin derivative. 24 Similar fragmentation patterns were observed for the precursor ions m/z 909 (22), 747 (29) and 601 (30). 37,40,41 The second-order mass spectra of the precursor ions of m/z 1087 (18), 793 (19), 925 (24), 895 (25) and 631 (26) showed the product ion Y 0 − at m/z 455, which corresponds to the deprotonated aglycone [A−H] − of the oleanolic acid ( Figure 4, Table 1).…”
Section: The Analysis Of the Ms/ms Mass Spectra Of The Precursor Ions Ofsupporting
confidence: 74%
“…In these compounds, peaks correspondent to the loss of a methyl galloyl moiety [M-H-168] − or a galloyl moiety [M-H-152] − , was also detected. Therefore, the compounds were assigned as tricin C -methylgalloyl glucuronide and tricin- C -galloyl- O -hexoside, respectively [70,71].…”
Section: Resultsmentioning
confidence: 99%
“…The spectra of flavonoids and phenolic acids have clear signals at ca. 340 or 270 nm [31,32]. For example, flavonols, most commonly in the form of glycosides, show absorbance maxima in the wavelength range from 260 to 355 nm.…”
Section: Spectroscopic Analysis Of Raw Materialsmentioning
confidence: 99%