Abstract:Today, sintering considers one of the significant processes that can be used in powder technology to produce a new solid product from powders using thermal energy. Many parameters can be successfully controlled by this process such as temperature, Particle size, process time, structure geometry, powder density, and powder composition. Study and analysis of the behavior of powder during the sintering process was carried out using finite element methods. The simulation provides two styles of discrete method and … Show more
“…The validation of published investigations is mostly based on the comparison to analytical findings, such as equation (2). 17 Moreover, these methods have rarely been applied to real microstructures yet.…”
Shrinkage during the sintering of powder compacts depends on numerous parameters, including green body characteristics such as particle size and green density. These parameters are also decisive for the initial microstructure and its evolution during sintering. In this study, a novel experimental setup is used to quantify the time-dependent microstructural evolution in water-atomised Astaloy 85Mo powder. Green bodies with different particle sizes and density levels were polished on the top surface and then subjected to an interrupted sintering procedure in a quenching dilatometer. Intermediate examinations of the microstructure by scanning electron microscopy revealed the pore morphology and the thermally etched austenite grain size. It was found that pore rounding relies solely on the local curvature only, whereas neck growth is in good agreement with analytical models. An increase in diffusivity was found on the macroscale and on the microscale due to the pre-deformation of the particles.
“…The validation of published investigations is mostly based on the comparison to analytical findings, such as equation (2). 17 Moreover, these methods have rarely been applied to real microstructures yet.…”
Shrinkage during the sintering of powder compacts depends on numerous parameters, including green body characteristics such as particle size and green density. These parameters are also decisive for the initial microstructure and its evolution during sintering. In this study, a novel experimental setup is used to quantify the time-dependent microstructural evolution in water-atomised Astaloy 85Mo powder. Green bodies with different particle sizes and density levels were polished on the top surface and then subjected to an interrupted sintering procedure in a quenching dilatometer. Intermediate examinations of the microstructure by scanning electron microscopy revealed the pore morphology and the thermally etched austenite grain size. It was found that pore rounding relies solely on the local curvature only, whereas neck growth is in good agreement with analytical models. An increase in diffusivity was found on the macroscale and on the microscale due to the pre-deformation of the particles.
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