ZnO-Al2O3 nanocomposite was synthesized and developed as a high performance sensitive and selective layer for surface acoustic wave (SAW) sensor, aiming for in-situ detection of H2S gas in ppb level operated at room temperature. ZnO-Al2O3 nanocomposite, synthesized though a sol-gel method, was spin-coated onto a quartz based SAW resonator. This composite layer inherits the mesoporous structure of the Al2O3 layer and good affinity to H2S gas molecules of the ZnO layer, and thus can selectively adsorb and react with H2S gas molecules to form ZnS compounds on its surface. This reaction leads to significant decreases of both pore sizes and total pore volume of the layer, an increase of layer's elastic modulus, thus causing a large positive shift of the frequency responses of the SAW sensor. The sensor operated at room temperature shows a frequency response of ~500 Hz to 10 ppb H2S, with an excellent selectivity and good recovery property.
In this letter, we propose a novel multiwavelength fiber laser based on fiber loop mirror formed by a highbirefringence fiber, a polarisation controller, and a 3 dB directional coupler. By setting the polarisation controller as half-waveplate, the fiber loop mirror acts as a polarisation-independent wavelength filter; Erbium-doped fiber (EDF) cooling by liquid nitrogen acts as gain medium. The wavelength spacing between the adjacent modes of the laser can be varied accurately by adjusting the length of the High-Birefringence (HiBi) fiber.
We report that cellulose nano-crystals (CNCs) can be used as a sensitive and selective layer in surface acoustic wave (SAW) sensors for in-situ HCl gas detection. CNCs were prepared through directly hydrolysis of cotton fiber and were spin-coated on quartz SAW resonators to form the sensitive layer. The CNCs have been identified to have abundant hydroxyl groups on their surfaces, which can act as the perfect adsorption sites for H2O, which can further act as the active sites for HCl gas adsorption. The absorption of HCl on the CNCs layer, thus leads to an increase of its mass, causing negative responses of the SAW sensors. Ambient humidity and thickness of CNCs layer are found to have significant influences on the responses of the SAW sensor. With an 80-nm-thick CNCs layer, the sensor shows a response of -2 kHz to 1 ppm HCl at 25 °C and relative humidity of 50% with an excellent selectivity and recovery characteristics.
A highly conductive three-dimensional (3D) graphene network (GN) was fabricated by chemical vapor deposition on a 3D nickel fiber network and subsequent etching process. Then a lightweight and flexible polydimethylsiloxane (PDMS)/GN composite was prepared by a vacuum infiltration method by using the graphene network as a template. The composite showed the superior electrical conductivity of 6100 S/m even at a very low loading level of graphene (1.2 wt %). As a result, an outstanding electromagnetic interference (EMI) shielding effectiveness (SE) of around 40 and 90 dB can be achieved in the X-band at thicknesses of 0.25 and 0.75 mm, respectively, which are much higher than most of the conductive polymers filled with carbon. The 3D graphene network can also act as a mechanical enhancer for PDMS. With a loading level of 1.2 wt %, the composite shows a significant increase by 256% in tensile strength.
An
ultrasensitive nitric oxide (NO) gas sensor based on the graphene
oxide (GO)-coated long-period fiber grating (LPFG) was constructed
successfully because of its excellent sensitivity to the surrounding
refractive index (SRI) change. The surface morphology and structure
of GO coated on LPFG were characterized by the scanning electron microscope
(SEM), scanning probe microscope (SPM), and Raman spectroscopy, respectively.
The adsorption principle of NO molecules by GO was calculated in detail
by density functional theory (DFT) and further characterized by Fourier
transform infrared spectrometry (FT-TR) and X-ray photoelectron spectroscopy
(XPS). Our studies demonstrate that the adsorption principle of NO
molecules by GO was the combined effect of physical adsorption and
chemical adsorption because of the formation of C–N bonds between
GO and NO and the oxidization of NO to NO2. The NO sensor
exhibits excellent sensing performance in the NO concentration range
of 0 to 400 ppm.
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