This study compared commercial composite resin blocks with one ceramic block for use in computer-aided design/computer aided manufacturing (CAD/CAM). Four composite resins, one composite ceramic, and one feldspar-ceramic block were investigated. Flexural strength (FS), flexural modulus (FM), and Vickers hardness (VH) were determined under three conditions: dry storage; immersion in water at 37°C for 7 days; and immersion in water at 37°C for 7 days followed by 10,000 thermocycles. After dry storage, FS ranged from 127 to 242 MPa, FM from 9.6 to 51.5 GPa, and VH from 64 to 455. Two-way ANOVA was performed for FS, FM and VH followed by Tukey's multiple comparison (α<0.05). Results demonstrated that the materials degraded after water immersion and thermocycling, but their properties were within the acceptable range for fabrication of single restorations according to the ISO standard for ceramics (ISO 6872:2008).
Gluma Dentin Bond is an adhesive system, where the primer contains 5% glutaraldehyde and 35% hydroxyethyl methacrylate. Practitioners have reported a strong desensitizing effect of the Gluma system on dentin. This study, thus, sought to evaluate the effect of this system on dentin using various microscopic techniques. 12 non‐restored human molars extracted for prosthodontic reasons were used. Prior to extraction the buccal cusps were removed such that a 2 mm × 2 mm wide dentin surface was exposed. The surfaces were treated in 6 ways: (1) application of Gluma 2 cleanser, Gluma 3 primer to which 0.1% w/v fluorescein was added, and Gluma 4 sealer; (2) as in (1) but treatment with H2O/0.1% w/v fluorescein instead of the Gluma 3; (3) as in (1) but without Gluma 2; (4) as in (1) but with application of 5% glutaraldehyde instead of Gluma 3; (5) as in (1) but without Gluma 4; (6) as in (1) but with application of 35% HEMA/0.1% w/v fluorescein instead of Gluma 3. Following extraction, 1 tooth per procedure was prepared for confocal laser scanning microscopy. The remaining teeth were fixed and prepared for SEM and TEM evaluation. In specimens of procedures (1) and (5), tubular occlusions could be seen to a depth of 200/μm. In specimens of procedure (4) tubular occlusions were found only to a depth of 50 μm. Such occlusions were not seen in control specimens (2), in specimens where the smear‐layer had not been removed (3), or following application of HEMA alone (6). It is concluded that glutaraldehyde can intrinsically block dentinal tubules. The septa in the tubules may counteract the hydrodynamic mechanism for dentinal sensitivity.
Nanofiller-containing resin composites have gained appreciable market share in dentistry due to their claims of high mechanical strength and low polymerization contraction. In this study, the polishability of one nanofill (Filtek Supreme XT/FIL) and three nanohybrid materials (Grandio/GRA, Tetric EvoCeram/TET, Venus Diamond/VED) was investigated using surface profilometry and SEM. After the specimens were cured under a Mylar strip or pre-ground with 600-grit SiC paper, three polishing systems were applied and their polishing effects compared: diamond polishing points, a diamond paste, and urethane-backed aluminum oxide disks. Except for the profilometry results obtained by glass filler-containing GRA and VED with one polishing system that comprised the consecutive application of diamond particles and a diamond polishing paste, the final roughness (Ra) of all other specimens were lower than the clinically acceptable 0.2 µm threshold. The surface textures of the polished nanofill FIL and nanohybrid TET were uniformly smooth, whereas relief polishing effects and filler extrusion of varying extents were seen on the nanohybrid composites GRA and VED.
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