We report on wafer-level measurements of the long-term stability of Ti and Ni ohmic contacts to n-4H-SiC during thermal treatments in air or air/moisture environments up to 500°C. Contact metallizations with and without a sputtered Ti (20 nm)/TaSi x (200 nm)/Pt (150 nm) diffusion barrier stack and Ti (20 nm)/TiN (10 nm)/Pt (150 nm)/Ti (20 nm) interconnects were compared. A protective coating consisting of a SiO x (250 nm)/SiN y (250 nm) stack deposited by plasma-enhanced chemical vapor deposition (PECVD) was used. The stability of the contact metallizations during long-term thermal treatments in air and air/moisture was studied. The best performance was achieved with Ti ohmic contacts without the Ti/TaSi x /Pt stack. This system successfully withstood 1000 h thermal treatment at 500°C in air followed by 1000 h at 500°C in air/10% moisture. After the aging, the contact failure ratio was below 1% and the specific contact resistivity amounted to (2.5 ± 1.1) 9 10 À4 X cm 2 . Scanning electron microscopy (SEM) cross-sectional analysis indicated no degradation in the contact metallization, demonstrating the effectiveness of the SiO x /SiN y protective coating in preventing oxidation of the contacts. These results are very promising for applications in harsh environments, where the stability of ohmic contacts is crucial.
In this work we present 4H-SiC metal-oxide-semiconductor field-effect transistors (MOSFETs) with a stable protective coating for harsh environment applications. Both inversion channel (IC) and buried channel (BC) MOSFETs were realized on n-4H-SiC substrates with a p-epilayer. Stacked ONO gate dielectric and Ti/TiN/Pt/Ti interconnect were used. Ni and Ti ohmic contacts in combination with a-SiOx/a-SiNy and a-SiOx/a-SiC protective coatings were compared. The MOSFETs showed excellent transistor characteristics up to 600 °C and exceptional stability during long-term aging at 600 °C in air and during accelerated aging at 700 °C including temperature cycling and air/moisture environment.
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