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ABSTRACTIn this paper, the compressive strength and in vitro bioactivity of sintered 45S5 bioactive glass scaffolds produced by powder technology and polymer foaming were investigated. The sintering temperature of scaffolds was 975°C. The characterization of scaffolds before immersion in SBF was performed by scanning electron microscopy (SEM) and microtomography (μCT). The scaffolds were also tested for compression, and their density and porosity were measured. After immersion, the samples were observed through SEM and analyzed using EDS, X-ray diffraction (XRD), and infrared spectroscopy (FT-IR). Mass variation was also estimated. The glass-ceramic scaffolds showed a 61.44 ± 3.13% interconnected porosity and an average compressive strength of 13.78 ± 2.43 MPa. They also showed the formation of a hydroxyapatite layer after seven days of immersion in SBF, demonstrating that partial crystallization during sintering did not suppress their bioactivity.
Bioactive glass 45S5 foams were produced as an alternative to be used to fill and restore bone deffects. A crucial design factor of foams is permeability, since it is related to their capability for waste removal and nutrients/oxygen supply to cells. In the present work a study was carried out to analyze the bioactive glass 45S5 foams permeability by Darcy’s law. The measure average permeability value on foams of 69-74 % porosity was 4.19 × 10-10, 3.75 × 10-10 and 3.48 × 10-10 m2, which are in the range of permeability values for trabecular bone.
RESUMENAndamios macroporos de biovidro 45S5 han sido desarrollados como una alternativa para sustituir injertos de hueso tradicionales. Un factor crucial en el diseño de estos andamios es la permeabilidad ya que de esto dependerá su capacidad para remover desechos y suministrar nutrientes y oxígeno a las células. En este trabajo se llevó acabo la evaluación de la permeabilidad basados en la ley de Darcy de andamios macroporos de biovidrio 45S5 con porosidades en el rango de 69%-74%. Los valores de permeabilidad obtenidos fueron de 4.19 × 10 -10 , 3.75 × 10 -10 y 3.48 × 10 -10 m 2 que estuvieron en el rango de los valores de permeabilidad del hueso trabecular.
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