ABSTRACT:The aim of this study was to evaluate the surface roughness, microhardness and morphology of human enamel exposed to six bleaching agents (at baseline and post-treatment). Human dental enamel samples were obtained from human third molars and randomly divided into seven groups (n = 11): control, Whiteness Perfect -10% carbamide peroxide (10% CP), Colgate Platinum -10% CP, Day White 2Z -7.5% hydrogen peroxide (7.5% HP), Whiteness Super -37% CP, Opalescence Quick -35% CP and Whiteness HP -35% HP. Bleaching agents were applied according to manufacturers' instructions. The control group remained not treated and stored in artificial saliva. Microhardness testing was performed with a Knoop indentor and surface roughness was analyzed with a profilometer. Morphologic observations were carried out with scanning electron microscopy (SEM). Results were statistically analyzed by two-way analysis of variance and Tukey's test (5%), and revealed a significant decrease in microhardness values and a significant increase in surface roughness post-bleaching. Changes in enamel morphology after bleaching were observed under SEM. It was concluded that bleaching agents can alter the microhardness, roughness and morphology of dental enamel surface.
Concern has been expressed regarding the adverse effects of peroxide-containing tooth bleaching agents on enamel surface. This study examined enamel average surface roughness before (baseline) and after an in-office bleaching protocol and investigated the influence of high concentrations of carbamide peroxide gels on its surface staining and morphology. Flat enamel surfaces were submitted to 35 and 37% % carbamide peroxide or to no bleaching treatment (n = 10) and evaluated with a profilometer. Eight specimens from each group were randomly selected and immersed in a 2% % methylene blue solution. Afterwards, specimens were ground into powder and prepared for the spectrophoto-metric analysis. Two remained specimens of each group were examined using a scanning electron microscope. Data were subjected to analysis of variance and Tukey test (P > 0AE05). Baseline roughness average was statistically similar for all groups, however, 35% % carbamide peroxide produced the roughest enamel surfaces. Different concentrations of carbamide peroxide produced similar staining means and enamel surface morphological alterations.
Aim: To evaluate the effects of activated charcoal powder (COAL) combined with regular (RT) or whitening (WT) toothpastes on enamel color and surface in comparison to carbamide peroxide (CP). Methods: Dental blocks (n = 10/group) were randomly divided into COAL, COAL/ RT, COAL/WT, CP, CP/RT, CP/WT, RT, WT, and CONT (without treatment). Simulated toothbrushing and whitening treatments were followed by colorimetric (ΔE 00 , L*, a*, b*), surface roughness (Ra), and enamel topography assays. ΔE 00 was submitted to two-way ANOVA and Tukey test. Color coordinates and Ra were tested with three-way repeated measures ANOVA (α = 5%). Results: COAL exhibited greater ΔE 00 than CONT (P = .048), but it did not enhance ΔE 00 promoted by RT or WT (P > .05). COAL alone increased Ra (P < .001) and altered enamel topography. COAL did not increase Ra caused by RT and WT (P > .05). CP exhibited the highest ΔE 00 (P < .05), but it raised Ra and changed enamel topography to a less extent than COAL. Conclusion: Even though charcoal powder did not increase enamel Ra when combined with toothpastes, the topography was negatively impacted by COAL. Also, COAL was unable to enhance the color change of RT and WT, or reach the effectiveness of CP. Clinical Significance: The use of activated charcoal-based product, claimed as a natural whitener, before brushing with toothpastes is not only ineffective to change the color of teeth, but also it might result in alterations on the enamel surface. Whitening with CP, instead, was effective during the same period of treatment, which still represents a more appropriate technique to whiten teeth.
Dentists should finish and polish composite resin with the polishing agent supplied by the same manufacturer. The smallest filler size does not necessarily result in a low surface roughness and staining susceptibility.
Concern has been expressed regarding the staining of enamel surface by different beverages after bleaching. This study investigated the influence of 35% hydrogen peroxide bleaching agents on enamel surface stained with wine after whitening treatments. Flat and polished bovine enamel surfaces were submitted to two commercially available 35% hydrogen peroxide bleaching agents or kept in 100% humidity, as a control group (n = 10). Specimens of all groups were immersed in red wine for 48 h at 37°C, immediately, 24 h or 1 week after treatments. All specimens were ground into powder and prepared for the spectrophotometric analysis. Data were subjected to two-way analysis of variance and Fisher's PLSD test at 5% significance level. The amount of wine pigments uptake by enamel submitted to bleaching treatments was statistically higher than that of control group, independently of the evaluation time. Results suggested that wine staining susceptibility was increased by bleaching treatments.
The goals of this study were to measure the water sorption (WS) and solubility (SO) of 3 composite resins containing different filler contents. Additionally, the size, shape, type and other characteristics of fillers were analyzed by scanning electron microscopy (SEM). Three composites, classified according to filler size, were selected: Filtek Supreme nanofill (3M/ESPE), Esthet-X minifill (Dentsply/Caulk) and Renamel microfill (Cosmedent Inc.). Ten disk-shaped specimens of each resin composite were made and stored in desiccators until constant mass was achieved. Specimens were then stored in water for 7 days, and the mass of each specimen was measured. The specimens were dried again and dried specimen mass determined. The WS and SO were calculated from these measurements. Data analyzed by one-way ANOVA and Tukey's post-hoc test (alpha=0.05). Composite filler particles were observed under SEM after removal of resin matrix by organic solvents. WS values were not significantly different among the resins; however, SO values were lower for Filtek Supreme. The materials presented differences in filler contents (e.g. particle size and shape). The composite resins had similar WS, while the SO was lower for the nanofill than for mini and microfill resins. The filler characteristics varied and were different among the materials.
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