Zn(II) complex of a newly synthesized ligand cyclododecanone thiosemicarbazone (CDDTSC) have
been synthesized and characterized by UV-visible spectroscopy, photoluminescence, X-ray diffraction,
scanning electron microscopy, EDX and transmission electron microscopy studies. Thermal
decomposition properties of the complex also were studied. The complex was subjected to thermal
decomposition in a high boiling solvent glycerol to get zinc sulphide nanoparticles. Highly crystalline,
mono-dispersed and well defined ZnS nanoparticles were obtained in good quantity, even in the absence
of capping agents.
Novel ligand (Cyclododecylidineamino)thiourea (CDDATU) and its Cadmium (II) complex were synthesized and characterized by IR, CHNS and Thermo gravimetric analysis.The complex was found to give highly crystalline, good quality, mono-dispersed Cadmium sulphide nanoparticles through polyol synthesis method using Glycerol as high boiling solvent. Characterization of Cadmium sulphide nanoparticles were done using SEM, EDX, TEM, UV, PL and PXRD studies.
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