To a considerable degree hardness is an empirical value which depends on many details involved in the measuring process. In the present work, hardness values were measured in the depth range 2 – 800 nm using microhardness, nanoindentation and scratch hardness tests on fused silica, steel and sapphire. It is shown that overestimation of hardness values for steel and sapphire with the nanoindentation method can be directly related to the relative height of pile-ups observed on the topography image of the indentation imprint. It is also shown that the scratch hardness test is a promising technique for nanoscaled hardness measurements.
The new procedure for the hardness measurements of superhard materials including diamond using the scanning force microscope with the ultrahard fullerite C60 tip was developed. It is shown that diamond is plastically deformed under the indentation by the ultrahard fullerite indenter at room temperature. Now the correct measurements of diamond hardness have become possible. The hardness values measured are 137 ± 6 and 167 ± 5 GPa for the diamond faces (100) and (111), respectively.
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