Pomelo (Citrus grandis .Linn Osbeck) oils is becoming more and more popular for everyone because it has great benefits. However, the efficiency of essential oil extraction process depends on the method and is influenced by a number of factors. Microwave-assisted hydro-distillation and Response Surface Methodology are selected for extracting and optimizing the factors affect the yield of the pomelo oil. The pomelo oil has the optimum yield was 4.5% when extracted with a water and peels ratio of 3,119: 1 (ml/g) for time extraction of 117.336 (minutes) at a microwave power of 403.115 (W) with high reliability (R2 = 0.9831)
Response Surface Methodology (RSM) is used to optimize the conditions of the saponification reaction (Concentration of alkaline solution (%), temperature (°C) and reaction time (hour)). Level of foaming and durability of the emulsion (cleaning ability) from the product of the saponification reaction are two factors to evaluate the optimization process by RSM. After optimization, the alkaline solution concentration is 11%, the reaction was carried out for 2.5-3 hours at 85°C for the highest level of foaming and the most prolonged durability of the emulsion. This parameter was compared with the experiment, and the results showed that there was no significant error, this proves that the RSM model has good repeatability, can optimally correct and is essential in optimizing the survey parameters.
Kaffir lime (Citrus hystrix D.C.), a member of the Citrus family, is a lemon tree naturally grown in tropical regions of Asia. Kaffir lime contains a specific aroma currently used worldwide as spices and cosmetics. Kaffir lime leaves are a famous spice for many dishes of Thai cuisine. The peel of Kaffir lime collected in the southwest of Vietnam was used for essential oil extraction using the process of hydro-distillation. During extraction, 100 g Kaffir lime peel was input at 1:3 ratio, at 120 °C for 90 min. The phytochemical profile of Kaffir Lime essential oil was analyzed by using gas chromatography/mass spectrometry (GC/MS) assay. The optimal essential oil yield reached 4.6%. A total of twenty-six components have been identified to account for 99.998% of essential oils. B-pinene (47.926%) was characterized as the main ingredient of peel oil. Other major components of Kaffir lime essential oil included D-limonene (24.121%), citronelal (11.84%), and α-pinene (2.834%). The present study evaluated the chemical compositions of Kaffir lime essential oil and compared with other previous studies. Future research on Kaffir lime EO can be expanded by using different extraction methods to improve its bioactive and applicability in many regions.
Coconut oil is considered the active ingredient as a moisturizer used by many people in tropical regions. At the same time, coconut oil can improve the symptoms of skin disorders by moisturizing and soothing the skin. A body washes formula that contains coconut oil based on the saponification process is formulated through an appropriate content survey. The combination of auxiliary substances such as detergent, foaming agent, moisturizing agent, preservative was also conducted to evaluate different concentrations. Products are assessed and visually observed for appearance, viscosity, pH value, stability, and durability when stored. The body wash formula was found to be white and pearl luster was visually observed. Products using 20% crude soap content, 5% detergent (SLES), 3% glycerin, etc. have all been tested to show good physico-chemical properties in terms of pH value and viscosity, as well as no irritation, upon skin contact. Research shows that coconut oil body wash formulas with good physico-chemical properties can be developed into new body wash cosmetic products.
Essential oils (EOs) are a complex element consisting of dozens to hundreds of compounds different. The essential characteristics of essential oils are governed by the main components of essential oils including oxygen monoterpen, hydrocarbon monoterpene, oxygen sesquiterpene, carbonylic compound, phenol, fatty acids and esters, which determine the primary aroma of essential oil. Kaffir lime EOs (Citrus hystrix DC; Rutaceae) is increasingly being used as a flavoring in perfume, cosmetic industries and food. Therefore, the purpose of this study is to extract essential oils from Kaffir lime to determine the components that create this fragrance. Kaffir lime EOs is obtained from 100g of fresh citrus peels of Citrus hystrix DC by microwave extraction method in 60 minutes and 450W power. The quality of Kaffir lime peel oil is assessed based on the chromatography of the compound present by the gas chromatography–mass spectrometry (GC-MS). Shell analysis led to the identification of twenty-six compounds that make up 100% of the essential oil and yield is 6%. The main compounds in kaffir lime shells such as β-pinene (45.206%), α-pinene (2.365%), D-limonene (18.358%), citronellal (17.745%), terpinen-4-ol (4.9964%).
Citrus hystrix which is commonly known as Kaffir Lime, is a plant with great potential for research and commercialization. C. hystrix essential oil is used as a fragrance to increase appetite in food, or sweet-smelling in cosmetics and antibacterial properties in the health field. Most research have focused on the peels, yet the EO content in C. hystrix leaves is also noteworthy. There are many essential oils extraction methods from conventional to advanced techniques. However, it is necessary to consider the influence of heat during heat transfer to constituents in materials, which easily decompose the volatile compounds contained in the essential oil. Steam distillation method can limit this disadvantage by separating the solvents and materials into two places that are only connected by a steam pipe. In this study, the steam distillation method was employed to extract the EOs from C. hystrix leaves. The chemical components in this EOs was evaluated by gas chromatography–mass spectrometry (GC-MS) method. C. hystrix leaves achieved an essential oil yield of 1.24%. Moreover, different compounds in Kaffir Lime EOs obtained from steam distillation method were identified, including β-citronellol, citronellyl acetate, linalool, caryophyllene, pinene, sabinene, and naphthalene. Findings from the present study provide helpful insights to effective essential oil extraction from C. hystrix leaves with high content of valuable phytochemical compounds.
Natural compounds have received much attention and research in recent years since the industrial economy developed. Essential oils, which contain many volatile constituents and aromatic compounds, have been around for a long time but are still considered to this day thanks to their natural properties and their unique application. There are several ways of collecting essential oils from herbal plants, including ancient approaches to contemporary techniques using different sections of plants such as buds, vegetables and nuts. In this study, the leaves of Kaffir lime (Citrus hystrix) were used to investigate the yield of essential oil extracted by the classical distillation system (hydro-distillation). The obtained essential oil was then analyzed for the chemical composition by gas chromatography–mass spectrometry (GC-MS). A total of 100 g of Kaffir lime leaves, under the following conditions: 1:3 of ratio of material to water, 120 °C of the temperature within 60 min. The extraction process yielded 1.3 mL of essential oils. GC-MS analysis also identified 16 compounds in the essential oil, accounting for 99.99% of total oils. The main compounds included citronellal (85.4%), citronellol (6.8%), linalool (1.9 %), citronellyl acetate (1.7%), and other compounds with content less than 1.0% by hydro-distillation. The findings of chemical composition of Kaffir lime leaves EO suggest further studies on optimization the extraction process for a desirable phytochemical content.
In recent years, essential oils extracted from different plant species have become increasingly popular in the production of pharmaceuticals, cosmetics, and foods. The essential oil from orange (Citrus sinensis) is important in large-scale applications due to its antibacterial, antioxidant activities, and pleasant aroma. In this study, factors affecting the production of orange essential oil on a distillation device with an operating capacity of 50 L/batch, including the ratio of material to water, temperature, and time distillation, have been surveyed. Through the survey, it was found that the raw materials were pureed, the materials: water ratio was 1:3 g/g, the water heating temperature was 130 °C, and the distillation time was 140 min. The yield of the essential oil was 1.8 mL/g with compounds limonene accounting for 98%, α-Pinene (0.655–0.734%), and β-Pinene (1.114 and 1.163%) by the GC-MS method. The review also found that the hydrodistillation equipment was designed to be suitable for the semi-industrial scales of orange essential oil due to its stable yield and volatile compounds contained in the essential oil.
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