Undoped and Mn doped ZnO samples with different percentage of Mn content (1 mol%, 2 mol% and 3mol%) were synthesized by a simple solvo-thermal method. We have studied the structural, chemical and optical properties of the samples by using x-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive x-ray (EDX) analysis, Fourier transform infrared (FTIR) spectroscopy and UV-VIS spectroscopy. The XRD spectra show that all the samples are hexagonal wurtzite structures. The lattice parameters calculated for the Mn doped ZnO from the XRD pattern were found to be slightly larger than those of the undoped ZnO, which indicates substitution of Mn in ZnO lattice. SEM photograph shows the grain size of undoped ZnO is bigger than the Mn doped ZnO's indicating hindrance of grain growth upon Mn doping. As the Mn doping increases the optical band gap decreases for the range of Mn doping reported here.
“Waste” Jute Fiber, an agricultural “waste” by-product was converted into an effective adsorbent and the same was tested for the removal of Malathion pesticide from aqueous solution. The prepared activated Jute fiber carbon (JFC) was characterized by using Scanning Electron microscope (SEM), X-ray diffractometer (XRD), Elemental analyzer and proximate analysis methods. Adsorption equilibrium, kinetics, thermodynamics and mass transfer studies were investigated as a function of agitation time, adsorbent dose, pH and temperature. The adsorption data obtained are found to obey Langmuir isotherm model. The adsorption kinetics was analyzed by using pseudo first order, pseudo second order and Elovich models. Thermodynamic parameters of adsorption process, i.e. ?G, ?S and ?H were computed and their negative values indicate the adsorption was exothermic and spontaneous nature.
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