The Fe3O4/Talc nanocomposite was synthesized by the coprecipitation-ultrasonication method. The reaction was carried out under a inert gas environment. The nanoparticles were characterized by X-ray diffraction (XRD), field-emission scanning electron microscopy (FESEM), fourier-transform infrared spectroscopy (FT-IR) and vibrating sample magnetometry techniques (VSM), the surface area of the nanoparticles was determined to be 77.92 m2/g by Brunauer-Emmett-Teller method (BET). The kinetic data showed that the adsorption process fitted with the pseudo-second order model. Batch experiments were carried out to determine the adsorption kinetics and mechanisms of Cr(VI) by Fe3O4/Talc nanocomposite. The adsorption process was found to be highly pH-dependent, which made the material selectively adsorb these metals from aqueous solution. The isotherms of adsorption were also studied using Langmuir and Freundlich equations in linear forms. It is found that the Langmuir equation showed better linear correlation with the experimental data than the Freundlich. The thermodynamics of Cr(VI) adsorption onto the Fe3O4/Talc nanocomposite indicated that the adsorption was exothermic. The reusability study has proven that Fe3O4/Talc nanocomposite can be employed as a low-cost and easy to separate.
In this study, Fe3O4/ZnO/chitosan magnetic nanoparticles were synthesized by an ultrasound-assisted coprecipitation method. The magnetic nanoparticles were characterized by XRD, FT-IR, FESEM, and VSM techniques. The effects of ultrasonication time and content of chitosan on crystal size and lattice parameters of the nanoparticles were also studied via XRD spectra. FESEM measurements revealed that the coating consists of Fe3O4/ZnO nanoparticles of 15-20 nm in diameter homogeneously dispersed on the surface of chitosan substance. The VSM measurements at room temperature showed that the Fe3O4/ZnO/chitosan nanoparticles had superparamagnetic properties. These results indicated that ultrasonication time and chitosan content had a significant effect on the characteristics of nanoparticles. The antibacterial activities of the Fe3O4/ZnO/chitosan were tested against both gram-positive Saccharomyces cerevisiae and Bacillus subtilis and gram-negative E. coli bacteria using a disk diffusion method.
In this study, the commercial organophosphorus compound Pyrovatex CP New was used as a flame retardant for cotton
fabric. Citric acid and a modified dihydroxy ethylene urea (DHEU) labelled Knittex FFRC were used as crosslinking to
increase the flame-retardant laundering durability of treated cotton fabric. There have been some studies showing that
Chitosan has the potential to improve flame retardancy and laundering durability of flame retardant treated cotton fabric.
Thus, Chitosan, which has the molecular weight of 2.600 (water soluble) and the deacetylation degree of approximately
75%, is added to finishing solution for flame retardant treatment of cotton fabric. The padding-drying-curing method was
used in this study. After treatment, all samples were examined to determine the chemical absorption level. The 45°
flammability test characteristics and LOI value of untreated and treated samples after different number of washing cycle
were determined to assess the flame retardancy of the treated fabric and its laundering durability. In addition, to assess
the impact of this treatment on the mechanical strength and ecology of the fabric, the tensile strength and free
formaldehyde content of the treated fabric were also evaluated
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