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This study aims to develop cavitation erosion-resistant clads on stainless steel (SS-316) using the microwave cladding technique. Ni-based alloy powder (EWAC) was reinforced with tungsten carbide (10% by wt) powder to obtain composite clads. The cladding process was carried out in a domestic microwave applicator of 2.45 GHz frequency with 900 W power. The microstructure, crystal structure (phase identification and quantification), and microhardness of the developed clad were investigated with scanning electron microscopy (SEM), energy-dispersive x-ray spectroscopy (EDX), x-ray diffraction (XRD), and Vickers microhardness tester, respectively. It was found that the deposited clad has a uniform thickness of ∼520 μm, and the microstructure mainly consists of equally dispersed and agglomerated carbides in cellular like Ni-Matrix. XRD analysis reveals that the composite clad was composed of various intermetallic, carbide, and oxide phases. The EWAC + 10WC clad (625 ± 81 HV0.3) has a hardness ∼3.5 times higher than the stainless steel substrate (195 ± 15 HV0.3). The cavitation erosion behavior of the SS-316 and EWAC + 10WC clad was examined by using a vibratory cavitation test apparatus. The parametric cavitation erosion testing was conducted according to the Taguchi L9 orthogonal array (OA) to study the effects of variations in amplitude (AMP), immersion depth (ID), and standoff distance (SOD) on mass loss in SS-316 and composite clad. The parametric study results show that SOD was the most influential test parameter, followed by AMP and ID. SOD contributes more than 50% in the mass loss of SS-316 and clad specimens, whereas AMP and ID contribution was around 32%–37% and 7%–11%, respectively. The developed EWAC + 10WC clad performed ∼6.7 times better than the SS-316. Nevertheless, the SS-316 and EWAC + 10WC clad specimens got severely damage in the form of pits, craters, plastic deformation, lip formation, impingement marks, and secondary cracks.

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Surface modification is one of the most reliable solutions for protecting the material damage in hydraulic turbines due to cavitation phenomena. However, the conventional coating/cladding process has many drawbacks like high porosity, weak adhesion strength, and poor fracture toughness. In contrast, the cladding process with microwave hybrid heating can overcome these limitations. Hence, this study aims to develop the microwave processed composite clad of Ni-based alloy with 40% Cr3C2 (by wt.) on SS-316 substrate in the domestic microwave oven of 2.45 GHz frequency and 900 W power. The selection of the material system for this study was based on mitigating the effect of cavitation erosion. The thorough metallurgical and mechanical characterization of the developed composite clad was done. Microstructural characterization using scanning electron microscopy revealed that the developed composite clads had a uniform thickness of 600 µm and free from interfacial cracks and visible pores (measured porosity ∼1.67% – as per ASTM B276). Uniformly dispersed hexagonal and stripe type carbides precipitate in the Ni-based alloy matrix of the composite clad was observed through scanning electron microscopy images. X-ray diffraction analysis shows that various hard carbides (SiC, Ni3C, Cr3Ni2SiC, Cr7C3, and NiC) and intermetallic (Ni3Fe, Ni2Si, and Cr3Si) phases were formed during microwave heating. The microhardness, flexural strength, fracture toughness of the Ni-40Cr3C2 clads were evaluated. The results reveal that the composite clad possesses microhardness = 605 ± 80 HV0.3 (∼3 times SS-316), flexural strength = 813.23 ± 16.2 MPa, and fracture toughness = 7.44 ± 0.2 MPa√m. The appropriate value of these properties makes this composite clad suitable for cavitation erosion resistance application.

Cavitation erosion is the primary cause of material failure of the hydroelectric power plant components. The rapid development in the advanced surface engineering techniques has provided an effective treatment solution for cavitation erosion. One such novel method is microwave cladding. Hence, the Ni–40Cr3C2 composite clad was deposited on austenitic stainless steel (SS-316) using a microwave cladding process in the present study. The processing was carried out in a domestic microwave oven of 2.45 GHz frequency and 900 W power. The developed clad was thoroughly characterized for the metallurgical and mechanical properties related to its behavior as a successful cavitation erosion resistance material, like microstructure, crystal structure, porosity, microhardness, flexural strength, and fracture toughness. The results showed that the stripe-type and agglomerated carbides were present in the Ni–40Cr3C2 clad. The developed composite clad consists of various carbides (SiC, Ni3C, Cr3Ni2SiC, Cr7C3, and NiC) and intermetallic phases (Ni3Fe, Ni2Si, and Cr3Si). Microhardness, flexural strength, and fracture toughness of the microwave-processed clad were observed to be 605 ± 80 HV0.3, 813.23 ± 16.2 MPa, and 7.44 ± 0.2 MPa√m, respectively. The microwave-processed composite clad performance in terms of cavitation erosion resistance was determined using the ultrasonic apparatus (ASTM-G32-17). The cavitation experiments were carried out according to Taguchi L9 orthogonal array, taking into account three parameters: standoff distance, amplitude, and immersion depth. The developed composite clad exhibited significant resistance (mass loss 7.6 times lesser as compared to SS-316) to cavitation erosion. ANOVA results showed the standoff distance as the most important factor followed by amplitude and immersion depth. Least cavitation resistance was observed at a smaller standoff distance, higher amplitude, and lower immersion depth. Linear regression equations were obtained to establish the correlation between parameters and cumulative mass loss. The microwave clad specimens tested at optimized test parameters were damaged in the form of fractured intermetallic, extruded lips, pits, and craters.

The current investigation aimed to study the cavitation erosion performance of the microwave synthesized NiCrSiC-5Al 2 O 3 composite clad with a 900 W power multimode domestic microwave applicator of 2.45 GHz frequency. The clads were deposited on the austenitic grade stainless steel, namely AISI-316. The as-deposited composite clad's microstructure, crystal structure, porosity, microhardness, and flexural strength were examined. Cavitation erosion study was done using the vibratory cavitation method at varying standoff distance (SOD)-(0.5 mm, 1 mm, 1.5 mm) and vibration amplitude (AMP)-(40 μm, 50 μm, 60 μm), keeping other parameters constant. The results had shown that the deposited NiCrSiC-5Al 2 O 3 composite clad exhibited 1.20% porosity, 489.16±47.95 HV 0.3 microhardness, 264.91±4.5 MPa flexural strength, and performed 3.5 times much better than the AISI-316 in terms of cavitation resistance. The least weight loss occurred at 1.5 mm SOD and 40 μm AMP, where the highest weight loss was observed at 0.5 mm SOD and 60 μm AMP. The erosion mechanism of the NiCrSiC-5Al 2 O 3 composite clad surface was observed as plastic deformation followed by surface fatigue; the clad surface was eroded in the form of pits, craters, impingement marks, secondary cracks, and plastically deformed lips.

Steel is the most commonly employed material in various engineering applications, and their successful machining demands finding the optimized set of machining parameters along with appropriate cooling strategies. Moreover, the significance of process parameter optimization is progressively perceived in the wake of expensive CNC machine adaptation on the shop floor for machining. Further, a competent cooling strategy is essential with a minimal amount of coolant to obtain the best quality products. In the present work, the optimization of process parameters for Near Dry Turning (NDT) of two steel grades, EN8 and EN31, was done. NDT utilizes a minimal coolant with a major amount of compressed air. For competent cooling, Al2O3 nanofluid as coolant was used with compressed air. Speed, feed, and depth of cut were taken as the machining parameters for the turning process. Two response variables, the surface roughness of machined specimen and cutting zone temperature, were considered for the analysis. Three levels of each turning parameter were chosen, and the Taguchi L9 orthogonal array was adopted for the experimentation. The optimized turning parameter was found through the Grey Relational Analysis (GRA). Further, the applicability of compressed air was also presented to achieve sustainable and green machining to eliminate the negative impact on environmental footprints. For this purpose, results at the obtained optimized set of parameters were compared with plain base fluid and compressed dry air as coolants. The reduction in surface roughness of ~12.3% and ~14.6% for EN8 and EN31 steel were observed using nanofluid in near dry turning. Similarly, the reduction in cutting zone temperature was ~7% in both cases. These results show the significance of process parameter optimization and the applicability of nanofluid in near dry turning of steels.

This work reports the comparison of heat-treated and non-heat-treated laminated object-manufactured (LOM) 3D-printed specimens from mechanical and morphological viewpoints. The study suggests that heat treatment of the FDM-printed specimen may have a significant impact on the material characteristics of the polymer. The work has been performed at two stages for the characterization of (a) non-heat-treated samples and (b) heat-treated samples. The results for stage 1 (non-heat-treated samples) suggest that the infill density: 70%, infill pattern: honeycomb, and six number of discs in a single LOM-manufactured sample is the optimized condition with a compression strength of 42.47 MPa. The heat treatment analysis at stage 2 suggests that a high temperature: 65 °C, low time interval: 10 min, works equally well as the low temperature: 55 °C, high time interval: 30 min. The post-heat treatment near Tg (65 °C) for a time interval of 10 min improved the compressive strength by 105.42%.