In this study, a novel route for the preparation of feedstock filaments for fused deposition modelling from recycled high-density polyethylene (HDPE) and low-density polyethylene (LDPE) waste polymers has been explored. For improving the properties of HDPE/LDPE-recycled polymers, Fe powder has been reinforced through single-screw extrusion. It has been observed that Fe powder (from 0 wt% to 25 wt%) in the LDPE and HDPE matrices has shown increasing trend in melt flow index. Furthermore, Fe powder reinforcement resulted in 36.66% improvement in hardness of reinforced HDPE polymer and 64% in LDPE. Mechanical properties (peak elongation, peak strength, break strength and shore D hardness (SDH)) have been improved significantly with the addition of 6 wt% and 10 wt% reinforcement of Fe powder in the matrix of LDPE and HDPE, respectively. The results of study suggest that morphological properties, such as SDH and percentage porosity, have direct relation with mechanical properties as it has been found that the sample with better mechanical properties was also having high hardness and low porosity. Scanning electron microscopy and energy-dispersive X-ray spectroscopy have been performed on 3D printed functional parts and it has been observed that highly dense texture of HDPE and low surface roughness resulted in better mechanical properties.
This paper reports properties of four different filaments prepared from (i) virgin polylactic acid, (ii) polylactic acid reinforced with polyvinyl chloride, (iii) polylactic acid reinforced with wood powder, and (iv) polylactic acid with reinforcement of Fe3O4 prepared with twin-screw extrusion for possible multimaterial three-dimensional printing. The results suggest that the melt flow rate of composite increases with the increase in reinforcements except for wood powder, which has shown a negative trend. Mechanical properties were also reduced with the loading but with the increase in the Fe3O4 content, these properties were improved. It has been observed that with reinforcement of polyvinyl chloride from 10 wt% to 25 wt% peak elongation and break elongation were reduced by 47.61% and 50%, respectively. Further, thermal analysis suggests that all samples were stable but for reinforced samples, the integral energy has decreased significantly in successive cycles. The vibration sample magnetometery of samples suggested that magnetic properties were dependent on the content of Fe3O4 present in the composite.
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