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Thermomechanical processing of low carbon bainitic steels is used to obtain a bainitic microstructure with good strength and toughness by continuous cooling after forging without the need of further heat treating, hence reducing manufacturing costs. However, hot forging parameters can significantly influence the microstructure in the forged material. A series of heat treating and forging experiments was carried out to analyze the effect of austenitizing time and temperature on the grain growth and the effect of forging temperature on the Prior Austenite Grain Size (PAGS) and continuously cooled microstructure. The forged microstructures were characterized by optical microscopy, microhardness tests, and X-ray diffraction. The results indicate that at 1200 °C austenitizing temperature abnormal grain growth takes place. Forging temperature significantly affects the PAGS and the subsequently formed microstructure. At high forging temperature (1200 °C), an almost fully bainitic microstructure was obtained. As the forging temperature was reduced to 1100 and 1000 °C, the PAGS refined, while the polygonal ferrite faction increased and the amount of retained austenite decreased. Further evaluations showed that a decrease in the forging temperature results in a higher carbon concentration in solution in the retained austenite leading to a stabilization effect.

The development of novel structural materials with increasing mechanical requirements is a very resource-intense process if conventional methods are used. While there are high-throughput methods for the development of functional materials, this is not the case for structural materials. Their mechanical properties are determined by their microstructure, so that increased sample volumes are needed. Furthermore, new short-time characterization techniques are required for individual samples which do not necessarily measure the desired material properties, but descriptors which can later be mapped on material properties. While universal micro-hardness testing is being commonly used, it is limited in its capability to measure sample volumes which contain a characteristic microstructure. We propose to use alternative and fast deformation techniques for spherical micro-samples in combination with classical characterization techniques such as XRD, DSC or micro magnetic methods, which deliver descriptors for the microstructural state.

The surface and subsurface conditions of components are significant for their functional properties. Every manufacturing process step changes the surface condition due to its mechanical, chemical and/or thermal impact. The depth of the affected zone varies for different machining operations, and is predetermined by the process parameters and characteristics. Furthermore, the initial state has a decisive influence on the interactions that lead to the final surface conditions. The aim of the investigation presented here is to compare the influence of the load characteristics over the depth applied to manufactured components by several different machining operations and to determine the causing mechanisms. In order to ensure better comparability between the surface modifications caused by different machining operations, the same material was used (AISI 4140; German steel grade 42CrMo4 acc. to DIN EN 10083-3) and annealed to a ferritic-pearlitic microstructure. Based on interdisciplinary cooperation within the collaborative research center CRC/Transregio 136 “Process Signatures”, seven different manufacturing processes, i.e., grinding, turning, deep rolling, laser processing, inductive heat treatment, electrical discharge machining (EDM) and electrochemical machining (ECM), were used, and the resulting surface zones were investigated by highly specialized analysis techniques. This work presents the results of X-ray measurements, hardness measurements and electron microscopic investigations. As a result, the characteristics and depths of the material modifications, as well as their underlying mechanisms and causes, were studied. Mechanisms occurring within 42CrMo4 steel due to thermal, mechanical, chemical or mixed impacts were identified as phase transformation, solidification and strengthening due to dislocation generation and accumulation, continuum dynamic recrystallization and dynamic recovery, as well as chemical reactions.

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