The fluorescence recovery after photobleaching technique (FRAP) was used to measure the diffusion coefficients (D) of fluorescein isothiocyanate (FITC)-dextrans in diluted, semidiluted, and concentrated hyaluronic acid solutions. The decrease of the diffusion coefficients as the hyaluronic acid concentration increases was consistent with the universal scaling equation D/Do = exp(-oc'). The diffusion experiments were carried out to obtain structural information on the transient network structure in hyaluronic acid solutions. On the basis of scaling laws, the concentration dependence of the average mesh size £ was determined as £ ~c-0•68*0•07. Additionally, the average £-values were estimated. The concentration dependence of £ and the absolute vlaues for £ were compared with structural information obtained from rheological experiments performed on hyaluronic acid solutions. Even though accurate results were found for the concentration dependence of £, there was a semiquantitative relation between the £-values estimated from the diffusion experiments and the rheological experiments.
This paper investigates textile-based energy storage devices fabricated with poly(3,4-ethylene dioxythiophene):poly(styrenesulfonate) (PEDOT:PSS) as an electro-active polymer and conductive yarns as the electrodes. The conductive yarns are sewn into a textile substrate and then coated with PEDOT:PSS systematically. Two different sets of devices were made. A comparison of the devices made with silver coated polybenzoxazol filament yarns and the devices made with pure stainless steel filament yarns is performed. The devices were charged and their self-discharge was measured by voltage decay. A study of the influence of charging time on the decay and the effect brought by various load resistors on the voltage decay is also performed. In this research, the devices with electrodes of pure stainless steel filaments yarns performed better than the devices with silver coated yarns; this outcome has been reported as standard by various researchers
The stability of wearable textile antennas after 20 reference washing cycles was evaluated by measuring the reflection coefficient of different antenna prototypes. The prototypes’ conductive parts were screen-printed on several textile substrates using two different silver-based conductive inks. The necessity of coating the antennas with a thermoplastic polyurethane (TPU) coating was investigated by comparing coated with uncoated antennas. It is shown that covering the antennas with the TPU layer not only protects the screen-printed conductive area but also prevents delamination of the multilayered textile fabric substrates, making the antennas washable for up to 20 cycles. Furthermore, it is proven that coating is not necessary for maintaining antenna operation and this up to 20 washing cycles. However, connector detachment caused by friction during the washing process was the main problem of antenna performance degradation. Hence, other flexible, durable methods should be developed for establishing a stable electrical connection.
Electrically conducting layers have been screen printed on woven textile substrates. Using the Van Der Pauw method for electrical resistivity measurements in thin layers, it was observed that the screen-printed layers showed anisotropic behavior. In order to be able to interpret the measurements correctly, a mathematical analysis of the measuring method has been established. From the experimental results one is then able to find the relation between the electrical resistivity in the warp versus the weft direction.
The thermal impedance Z th (jx) has been calculated numerically, using the boundary element method, for a silicon substrate with a uniform heat source on top. The key feature is that the dynamic thermal behaviour is calculated directly in the frequency domain. The calculations were performed for a wide range of values for the thickness of the substrate. By representing the thermal impedance in a Nyquist plot (i.e. Im[Z th (jx)] vs. Re[Z th (jx)] with x as parameter), mainly two circular arcs are observed. For the lower frequency arc, the impedance values as well as the frequency scale are found to be largely influenced by the substrate thickness. The arc corresponding to high frequencies on the other hand remains unchanged under thickness variations.Further analysis revealed an almost perfectly linear relationship between the thermal resistance R th = Z th (jx = 0) and the substrate thickness, even when the heat source is not centred on the substrate. Both the slope and intersection value obtained from the curve fitting can be explained by a simple geometrical model including the fixed-angle heat spreading approximation, used since many years in the literature.
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