The API 5L X70 steel is used in high-pressure gas transmission pipelines. Because of this, knowledge of presence of residual stress and their magnitude is important to assess the material integrity in service. For the pipeline manufacturing, tubes need to be curved which is often made using the hot induction bending process. This process can introduce different residual stress depending of tube position. For this research, in order to evaluate the residual stress, was used an API 5L X70 tube that was previously curved by hot induction process. Samples were taken from the extrados, intrados, neutral line and straight section of the curved tube. Residual stresses were studied by two conventional methods: X-Ray Diffraction (XRD) and Hole-Drilling, which are destructive and non-destructive methods, respectively, in order to assess their qualitative responses. Each of these methods presents particular methodologies in sample preparation and material analysis, but also they differ in factors such time consumption and cost of the analysis. The qualitative responses obtained by the two different methods were comparable and satisfactory and pointed out the existence of a compressive residual stress state in steel pipe.
Reducing pollutant emissions and improving safety standards are primary targets for modern mobility improvement. To meet these needs, the development of low-density steels containing aluminum is a new frontier of research for automotive applications. Low-density Fe-Mn-Al-C alloys are promising. In this regard, an alloy with high aluminum content and niobium addition belonging to the Fe-Mn-Al-C system was evaluated to understand the possible phase transformations and thus obtain a transformation diagram by continuous cooling to help future processing. Dilatometry tests were performed in a Gleeble thermomechanical simulator with different cooling rates (1, 3, 5, 10, 15, 20, 30, and 50 °C/s). Chemical analyses carried out simultaneously with dilatometry tests showed the presence of proeutectoid ferrite (αp), δ-ferrite, retained austenite, and niobium carbide (NbC). In the case of low cooling rates (1 and 3 °C/s), lamellar colonies of the eutectoid microconstituents were observed with a combination of α-ferrite and k-carbide. For higher cooling rates (5 to 50 °C/s), martensite was observed with body-centered cubic (BCC) and body-centered tetragonal (BCT) structures.
ResumoA textura cristalográfica e a densidade de discordâncias têm um papel importante nas propriedades de vários metais, podendo ser modificada de acordo com os processamentos mecânicos e tratamentos térmicos realizados, além disto, também é influenciada pela estrutura cristalina e energia de falha de empilhamento (EFE). O presente trabalho buscou observar a influência da EFE na textura cristalográfica e na densidade de discordâncias de metais CFC submetidos a laminação a frio. Os materiais usados foram o latão α, cobre e uma liga de alumínio 1050, que possuem baixa, média e alta EFE, respectivamente. Pode-se observar que diferentes níveis de EFE propiciaram, para a mesma redução da espessura após a laminação a frio, distintas texturas nos materiais utilizados e diferentes densidades de discordâncias. Palavras-chave: Textura cristalográfica; Energia de falha de empilhamento; Densidade de discordância; Metais CFC.
INFLUENCE OF THE STACKING FAULT ENERGY IN THE DISLOCATIONS DENSITY AND CRYSTALLOGRAPHIC TEXTURE OF FCC METALS AbstractThe crystallographic texture and the dislocations density has an important role in the metals properties and that can be evolved through the mechanical and thermal processing performed, and in addition is also affected by crystalline structure and the stacking fault energy (SFE). This study aimed to observe the influence of SFE in the crystallographic texture development and dislocation density of FCC metals subjected to cold rolling and posterior annealing. The materials used were α-brass, copper and 1050 aluminum alloy, which has low, medium and high SFE, respectively. It can be seen that for FCC materials with different levels of SPEs and same cold reduction, different textures and densities of dislocations were obtained which can be explained basis on the difference in SFE.
High Strength Low Alloy steels (HSLA) for oil and gas pipelines should display high mechanical strength, toughness, ductility and weldability. In this work we studied the influence of quenching and tempering temperature on the yield strength, ultimate tensile strength, percent elongation and hardness of API 5L steel pipes in order to optimize heat treatments to be performed after hot induction bending of the material. The thermal cycles involved soaking temperatures of 880, 920 and 960 °C, cooling water at 15, 23 and 31 °C and tempering at 530, 600 and 670 °C. From this, experimental design techniques were used to reduce the number of experiments. The results from contour maps suggest that soaking temperatures of 910 and 950 °C and tempering between 540 and 610 °C were the most suitable for treatment, regarding mechanical strength. The variation of the water temperature was not significant for the assumed cooling conditions. The prediction regression models of the mechanical properties from the variables involved in the heat treatments showed a good fit between the experimental and predicted results, with correlation coefficient between 0.89 and 0.94.
δ-TRIP steel is a recent concept and has been developed over the last ten years aiming to combine good mechanical strength and ductility. This class of steels is multiphase and contains δ and α ferrites, as well as austenite, bainite and/or martensite. The TRIP (Transformation Induced Plasticity) effect is influenced by those phases proportion, which depends on alloying contents. This paper investigates a chemical composition that allows adequate proportion among the phases, optimizing the microstructures by means of computational methods. These microstructures are designed to contain between 10 to 50% austenite, 10 to 70% α-ferrite and 20 to 80% δ-ferrite at the eutectoid temperature. The ThermoCalc Software [1] was used to predict the fractions of the microconstituents, producing graphs describing areas of interest of microconstituents as function of alloying elements variations that leads to the desired microstructure. Results indicate that the designed volume of the phases can be found for certain proportions among the alloying elements, higher concentrations of Al and Nb combined with C allow or not the occurrence of carbides and other phases in smaller quantities.
Resumo Os aços passíveis de efeito TRIP (Transformation Induced Plasticity) denominados de aços TRIP surgiram durante o desenvolvimento de aços com a finalidade de satisfazer as exigências da indústria automotiva, devido a seu mecanismo particular de deformação. Este trabalho avalia amostras de aços na condição forjada, em escala laboratorial, de distintas composições químicas com alto teor de alumínio e distintas adições de carbono e nióbio visando a produção de uma liga susceptível ao efeito TRIP, via microscopia óptica e análises de difração de raios X (DRX), a fim de verificar a homogeneidade e as fases presentes na microestrutura. Por meio das análises obteve resultados satisfatórios para as condições de alto e baixo carbono com adição de nióbio (A1 e B1). Palavras-chave: Aços TRIP; Caracterização microestrutural; DRX.
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