The thermal decomposition of the native GaSb oxides is studied using time resolved x-ray photoelectron spectroscopy with a temperature resolution of better than 1 K. The expected transfer of oxygen from Sb-O to Ga-O before the eventual desorption of all oxides is observed. However, an initial reaction resulting in the reduction of Sb 2 O 3 along with the concurrent increase in both Ga 2 O 3 and Sb 2 O 4 is detected in the temperature range of 450-525 K. Using the relative changes in atomic concentrations of the chemical species observed; the initial reaction pathway is proposed.
Due to the performance requirements of displays and lighting applications, there is a great need to measure the radiant flux and colour of light-emitting diodes (LEDs) simultaneously in a high throughput format. We evaluate the feasibility of obtaining reliable colour and radiant flux values of LEDs with a low-cost office flatbed document scanner under factory settings versus conventional measurements. Colour purity was evaluated against a spectrometer and a digital camera, while radiant flux was evaluated against photodiodes. Scanner colour rendition of red, green and yellow LEDs was of variable quality. The scanner showed better correlation to conventional radiant flux measurements, with linear least-squares agreement between 0.934 and 0.985. A scanner represents a low cost and high throughput means of evaluating LEDs with simultaneous measures of both electroluminescent flux and emission colour with operational time.
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