2017
DOI: 10.15587/1729-4061.2017.101071
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Usage of mother liquor recycling for the obtaining of Fe(VI) compounds

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“…The purity of K 2 FeO 4 was determined by chromite titration [28,29] and spectrophotometry by Specord 210 of Analytik Jena (Germany) as well as ion chromatography by Biorad IC-Anion-PW column (USA) to identify and quantitate impurity ions, chloride and nitrate. In the second series of experiments, solutions of ferrate(VI) in 8.0 M KOH were prepared by the electrochemical method [32,33]. These solutions are resulting from t=20 o C by electrochemical dissolution of steel plates (S=10 cm 2 ) containing: C -0.16 %; Mn -0.43 %; Si -0.04 %; S -0.03 %; P -0.04 %; the rest is Fe.…”
Section: Materials Substances and Devices Used For The Synthesis mentioning
confidence: 99%
“…The purity of K 2 FeO 4 was determined by chromite titration [28,29] and spectrophotometry by Specord 210 of Analytik Jena (Germany) as well as ion chromatography by Biorad IC-Anion-PW column (USA) to identify and quantitate impurity ions, chloride and nitrate. In the second series of experiments, solutions of ferrate(VI) in 8.0 M KOH were prepared by the electrochemical method [32,33]. These solutions are resulting from t=20 o C by electrochemical dissolution of steel plates (S=10 cm 2 ) containing: C -0.16 %; Mn -0.43 %; Si -0.04 %; S -0.03 %; P -0.04 %; the rest is Fe.…”
Section: Materials Substances and Devices Used For The Synthesis mentioning
confidence: 99%