The High Temperature Equilibrium of Titanium Dioxide and Carbon With Titanium Carbide and Carbon Monoxide

Brantley, L. Reed; Beckman, Arnold O.

doi:10.1021/ja01373a026

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Tio Preparation1

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1933

2013

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Cited by 17 publications

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“…Others (40) prepared TiO in a like manner, but were unable to confirm the formation of TiO as a solid phase by the reduction of TiO~ with carbon. Junker (41) also assumed that the reduction of TiO2 with carbon merely yields mixtures of Ti203 and TiC.…”

Section: Tio Preparationmentioning

confidence: 99%

Electrolytic Reduction of Titanium Monoxide

Sibert¹,

Mckenna²,

Steinberg³

et al. 1955

J. Electrochem. Soc.

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An electrolytic method for preparation of titanium metal from titanium monoxide is described. The process is carried out in alkaline earth halide melts under an inert atmosphere. The inert atmosphere cell and its operation are described. Methods for preparation of reduced titanium oxides are also discussed. These include reactions of titanium carbide with ZnO or MgO, carbon reduction of TIP2, and electrolytic reduction of TIP2. Electrolytic titanium prepared from TiP is deposited as a crystalline metal powder in a salt matrix and is recovered by aqueous techniques. Although metal so prepared has not generally been acceptable from a purity standpoint, revision in cell design and procedure could offer improvement in this respect.

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Section: Tio Preparationmentioning

confidence: 99%