2018
DOI: 10.4314/bcse.v31i3.8
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Synthesis of Schiff bases derived from 2-hydroxy-1- naphth- aldehyde and their tin(II) complexes for antimicribial and antioxidant activities

Abstract: ABSTRACT.The current studies were designed to prepare tin(II) complexes of various Schiff base derivatives of 2-hydroxy-1-naphthaldehyde (HN) with L-histidine and sulfamethazine have been prepared and characterized by different physiochemical studies such as elemental analysis, atomic absorption, UV-Vis spectra, FTIR spectra, 1 H-NMR, 13 C-NMR and conductance studies. Antimicrobial and antioxidant activities were also calculated. Antibacterial activity was evaluated by the agar-well diffusion method. Two Gram-… Show more

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Cited by 29 publications
(13 citation statements)
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“…The azomethine and phenoxy carbon signals resonated at δ = (157.72–151.97) and δ = (156.29–116.28) ppm, respectively ( Supplementary file Figures S17, S19 and S21 ). The presence of azomethine proton and a carbon signals were in concord with the reports from various literature confirming the successful synthesis of Schiff bases 1 – 9 [ 39 , 40 ].…”
Section: Discussionsupporting
confidence: 86%
“…The azomethine and phenoxy carbon signals resonated at δ = (157.72–151.97) and δ = (156.29–116.28) ppm, respectively ( Supplementary file Figures S17, S19 and S21 ). The presence of azomethine proton and a carbon signals were in concord with the reports from various literature confirming the successful synthesis of Schiff bases 1 – 9 [ 39 , 40 ].…”
Section: Discussionsupporting
confidence: 86%
“…Stronger antioxidants can reduce absorbance rapidly. The IC 50 value, defined as the concentration of the sample causing the DPPH concentration to be reduced by 50%, is calculated from the linear regression of the concentration graphs of the compounds tested against the mean percentage of antioxidant activity [123,124]. The lower the IC 50 value, the higher the antioxidant activity of the tested samples.…”
Section: Antioxidant Activity Resultsmentioning
confidence: 99%
“…Which is in the usual range of reported Schiff base complexes. 39 The 1 H-NMR spectrum of ligand E exhibited a singlet peak at δ 2.5 ppm is assigned to (-CH 2 -Br) group attached to azomethine group when the other peaks which appeared around δ 7.47-8.13 ppm is attributed to fourteen aromatic rings.…”
Section: Nmr Spectral Analysismentioning
confidence: 96%