2006
DOI: 10.1111/j.1365-2818.2006.01664.x
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Structural analysis and intergranular corrosion tests of AISI 316L steel

Abstract: SummaryPure AISI 316L steel is investigated after solution heat treatment (1050 °C/H 2 O) and structural sensitization (650 °C). Two quite different intergranular corrosion tests are used to determine the degree of structural sensitization due to the precipitation of secondary phases along the grain boundaries (mainly the M 23 C 6 and σ-phase): the oxalic acid etch test and the electrochemical potentio-kinetic reactivation test. Generally, the dissolution of chromium-rich carbides (M 23 C 6 ) is provoked by ox… Show more

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Cited by 9 publications
(7 citation statements)
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“…The results of EPR-DL showed that ASIS 316L manufactured by SLM indicates minor signs of grain boundary sensitization, and it was confirmed that both heat treatment strategies used even improved intergranular corrosion resistance. Previous studies performed on continuously casted AISI 316L [74,75] revealed significant grain boundary sensitization after heat treatment at 650 • C/H 2 O due to the precipitation of chromium-rich secondary phases along the grain boundaries (mainly the M 23 C 6 and σ-phase). The exact opposite effect was confirmed for additively manufactured material heat treated at the same temperature used for research in this paper.…”
Section: Discussionmentioning
confidence: 96%
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“…The results of EPR-DL showed that ASIS 316L manufactured by SLM indicates minor signs of grain boundary sensitization, and it was confirmed that both heat treatment strategies used even improved intergranular corrosion resistance. Previous studies performed on continuously casted AISI 316L [74,75] revealed significant grain boundary sensitization after heat treatment at 650 • C/H 2 O due to the precipitation of chromium-rich secondary phases along the grain boundaries (mainly the M 23 C 6 and σ-phase). The exact opposite effect was confirmed for additively manufactured material heat treated at the same temperature used for research in this paper.…”
Section: Discussionmentioning
confidence: 96%
“…This resulted in an increasing of chromium volume content along grain boundaries and their possibility of spontaneous repassivation, even under conditions of aggressive sulfuric acid solution used for testing [77]. The indisputable fact is that powders used for the SLM method contained considerably lower carbon content than material used for experiments presented in studies: [74,75], which resulted in a reduced amount of chromium-rich carbide precipitated along grain boundaries, causing a less significant change of chromium dissolved in solid solution.…”
Section: Discussionmentioning
confidence: 99%
“…Under certain conditions, the precipitation of intermetallic compounds of (Fe, Cr)Mo 2 or (Cr, Ni, Fe) 3 P 2 type can occur. According to Stonawská et al, the structural sensitization of 316 L steel is due to the precipitation of secondary phases along the grain boundaries [59]. The studies of Liu et al regarding 316 L steels [60] and Fujii et al [61] regarding 304 steel, also supports this statement.…”
Section: #750_2mentioning
confidence: 90%
“…Ketika baja tahan karat austenitic terpapar dalam waktu yang lama pada suhu antara 500 dan 850 o C terjadi proses presipitasi karbida. Sejumlah besar fase selain Cr 23 C 6 terbentuk antara lain Cr 6 C dan fase sigma, fase intermetalik chi dan laves [3]. Fase sigma yang terbentuk memiliki kandungan kromium dan molybdenum yang lebih tinggi dibandingkan dengan fase austenite sehingga presipitasi di batas butir menyebabkan deplesi unsur-unsur tersebut pada bagian matriksnya.…”
Section: Pendahuluanunclassified