This paper deals with the investigation of complex corrosion properties of 3D printed AISI 316L steel and the influence of additional heat treatment on the resulting corrosion and mechanical parameters. There was an isotonic solution used for the simulation of the human body and a diluted sulfuric acid solution for the study of intergranular corrosion damage of the tested samples. There were significant microstructural changes found for each type of heat treatment at 650 and 1050 °C, which resulted in different corrosion properties of the tested samples. There were changes of corrosion potential, corrosion rate and polarization resistance found by the potentiodynamic polarization method. With regard to these results, the most appropriate heat treatment can be applied to applications with intended use in medicine.
The contribution is aimed at corrosion propertied and wettability of basic graded of stainless steel commonly used in medicine as a standard for construction of instruments and other applications. Samples of AISI 304 (1.4301) steel were chemical passivated by nitric acid and tested for corrosion resistance in environment of sodium hypochlorite (NaClO), which is commonly used for basic disinfection of surfaces or devices in hospital facilities. It was found that chemical passivation of stainless steel surface increases its corrosion resistance and lower corrosion rate. Passivation layer also shows more polarization resistance. The wettability of passivated surface was measured by sessile drop method. Wettability itself determinates effectivity of disinfection process as the surfaces with lower contact angle may be cleaned and disinfected with more efficiency. It was proofed that chemical passivation increases wettability by lowering contact angle of treated surface.
In this paper corrosion properties and microstructure features of amorphous self-organised TiO2 nanotubes electrochemically deposited on titanium are discussed. There was titanium of second grade used as a substrate for these experiments. There was a specific solution of ammonium fluoride, ethylenglycol and deionized water used to create an oxide layer with advantageous properties. Relation between changes of roughness indexes before and after anodization was found out. The wettability (contact angle) of artificial plasma on surface was measured using sessile drop method. It was found out that titanium dioxide nanotubes formed on the surface significantly decreases contact angle and time of anodization reduces it even more. Corrosion potentials, corrosion rate or polarization resistance were determined by linear polarization methods performed by ASTM standards. Corrosion potential of anodized samples is substantially more positive (≈ -50mV) compared with non-treated sample (≈ -280mV). On the other hand polarization resistance was significantly higher for non-treated sample. Also potentials of passive layer breakdowns were found. Structure of nanotubes and influence of anodization on surface profile was studied by SEM.
The presented article investigates the biomechanics of the calcaneal nail C-NAILTM by numerical calculations and, partially, experimentally. This nail is widely used in trauma and orthopaedics. A numerical model of implants directly interacting with the bone tissue model obtained from CT scans was calculated. The material properties of the bone tissue can be described by several models; in this work, a non-homogeneous material model with isotropic elements and prescribed elastic modulus was used to provide a more accurate model of the applied force distribution on the individual parts of the implants. The critical areas of the nail and its fixtures were investigated using finite element strength calculations to verify their strength and reliability, contributing to the safety and faster and easier treatment of patients. These analyses suggest that the strength of the calcaneal nail C-NAIL, as well as the stabilization of bone fragments resulting from its use, are sufficient for clinical practice.
The topic of the article concerns the mechanics of machining plastics and their machined surface. This article deals with measurements and their stochastic (probabilistic) evaluation of the force and moment loading of the machine tools and workpiece. It also deals with the quality of the machined surface in relation to its surface roughness and surface integrity. Measurements were made under different cutting conditions on a CNC milling machine using a newly designed cutter with straight teeth. The statistical evaluation is presented by bounded histograms and basic statistical characteristics that give a realistic idea of the machining process. The practical focus of the experiments is on the milling of HPL (high-pressure plastic–laminate composite material). The listed procedures can also be applied to other materials and machining methods, and can be used for numerical modelling, setting the optimum parameters of machining technology, or for the design of cutting tools. Numerical modelling and other solution options are also mentioned. We have not yet found detailed information in the literature about the milling of HPL material, and our results are therefore new and necessary.
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