Soxhlet-assisted matrix solid phase dispersion to extract flavonoids from rape (Brassica campestris) bee pollen

Ma, Shuangqin; Tu, Xijuan; Dong, Jiangtao; Peng, Long; Yang, Wenchao; Xing, Miao; Chen, Wenbin; Wu, Zujian

doi:10.1016/j.jchromb.2015.09.038

Cited by 12 publications

(11 citation statements)

References 37 publications

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“…Slight decreases in extraction yields were found when the mass ratio was increased to 1:3 and 1:4. This influence was also observed in the SA‐MSPD (Ma et al , ), and may be due to the enhanced retention of flavonoids in the larger mass of solid support. Compared to the control experiment (Fig.…”

Section: Resultssupporting

confidence: 54%

“…The MSPD performance also improves the extraction yield. Silica gel has been shown to be a suitable solid support for the extraction of flavonoids in SA‐MSPD (Ma et al , ). The effect of mass of silica gel on the extraction yields is shown in Fig.…”

Section: Resultsmentioning

confidence: 99%

“…MSPD is an effective sample preparation technique for the extraction of bioactive compounds from plant materials (Capriotti et al , ; Dawidowicz et al , ; Yin et al , ; Visnevschi‐Necrasov et al , ). In a recent study (Ma et al , ), we developed a modified MSPD method named Soxhlet‐assisted matrix solid phase dispersion (SA‐MSPD) for the extraction of flavonoids from bee pollen, which is a flavonoid‐rich honeybee product (Bonvehí et al , ). Maceration extraction (ME) (Feás et al , ; Lv et al , ) and ultrasonic‐assisted extraction (UAE) (Tao et al , ; Zhou et al , ) have been used for the extraction of flavonoids from bee pollens.…”

Section: Introductionmentioning

confidence: 99%

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One-Step Extraction and Hydrolysis of Flavonoid Glycosides in Rape Bee Pollen Based on Soxhlet-Assisted Matrix Solid Phase Dispersion

Gao

et al. 2017

Phytochem. Anal.

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The proposed methodology is simple and highly efficient, with good repeatability and recovery. Compared with currently available methods, the present work has advantages of using less time and labour, higher extraction efficiency, and less consumption of the acid catalyst. This method may have applications for the one-step extraction and hydrolysis of bioactive compounds from plant materials. Copyright © 2017 John Wiley & Sons, Ltd.

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Section: Resultssupporting

confidence: 54%

Section: Resultsmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

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One-Step Extraction and Hydrolysis of Flavonoid Glycosides in Rape Bee Pollen Based on Soxhlet-Assisted Matrix Solid Phase Dispersion

Gao

et al. 2017

Phytochem. Anal.

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“…To further investigate the practicability of the proposed method, a comparison with other methods existed for flavonoid extraction was performed in terms of extraction method, solvent, extraction time, analysis method and time (Table ). It was found that these reported methods required frequently a large amount of sample (more than 0.5 g) and extraction solvent (more 10 mL) while the current industrial MCM‐41‐MMSPD extraction method only required the milligram amounts of sample (25 mg) and reagent (1.25 mL) . In addition, most of these methods mainly focused on a few flavonoids or total flavonoids, which were insufficient for evaluation quality of TCMs with multi‐compounds.…”

Section: Resultsmentioning

confidence: 99%

A rapid and efficient extraction method based on industrial MCM‐41‐miniaturized matrix solid‐phase dispersion extraction with response surface methodology for simultaneous quantification of six flavonoids in Pollen typhae by ultra‐high‐performance liquid chromatography

Wang

Yang

et al. 2019

J of Separation Science

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An industrial MCM-41-miniaturized matrix solid-phase dispersion extraction coupled with response surface methodology was explored to determine L-epicatechin, typhaneoside, isorhamnetin-3-O-neohespeidoside, naringenin, kaempferol, and isorhamnetin in Pollen typhae by ultra-high performance liquid chromatography connected to a photodiode array detection. Several variables were optimized in detail, including mesh number of sieve, type of adsorbent, mass ratio of sample to adsorbent, grinding time, methanol concentration, and elution volume. Central composite design was applied to optimize the best conditions for the maximum yields of the total flavonoids. The results displayed a good linear relationship (R > 0.9992) and the recoveries ranged from 92.9 to 103% (RSD < 4.53%) of the six flavonoids. The optimal method with high efficiency and low consumption was obviously better than heating reflux and ultrasonic extraction. It was proven that the developed industrial MCM-41-miniaturized matrix solid-phase dispersion extraction coupled with simple ultra-high performance liquid chromatography method could be a rapid and efficient tool for extraction and determination of flavonoids in natural products. K E Y W O R D SMCM-41, miniaturized matrix solid-phase dispersion extraction, response surface methodology, traditional Chinese medicine, ultra-high-performance liquid chromatography 2426 -x. A rapid and efficient extraction method based on industrial MCM-41miniaturized matrix solid-phase dispersion extraction with response surface methodology for simultaneous quantification of six flavonoids in Pollen typhae by ultra-high-performance liquid chromatography. J

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“…Recently, we reported the combination of Soxhlet extraction and MSPD to develop a Soxhlet assisted MSPD (SA-MSPD) method [ 60 , 61 ]. In this modification method, sample was blended with silica gel following the original MSPD protocol and loaded into a column of constant pressure funnel.…”

Section: Modification Of Original Mspdmentioning

confidence: 99%

A Review on the Recent Progress in Matrix Solid Phase Dispersion

Chen

2018

Molecules

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Matrix solid phase dispersion (MSPD) has proven to be an efficient sample preparation method for solid, semi-solid, and viscous samples. Applications of MSPD have covered biological, food, and environmental samples, including both organic and inorganic analytes. This review presents an update on the development of MSPD in the period 2015~June 2018. In the first part of this review, we focus on the latest development in MSPD sorbent, including molecularly imprinted polymers, and carbon-based nanomaterials etc. The second part presents the miniaturization of MSPD, discussing the progress in both micro-MSPD and mini-MSPD. The on-line/in-line techniques for improving the automation and sample throughput are also discussed. The final part summarizes the success in the modification of original MSPD procedures.

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Soxhlet-assisted matrix solid phase dispersion to extract flavonoids from rape (Brassica campestris) bee pollen

Cited by 12 publications

References 37 publications

One-Step Extraction and Hydrolysis of Flavonoid Glycosides in Rape Bee Pollen Based on Soxhlet-Assisted Matrix Solid Phase Dispersion

One-Step Extraction and Hydrolysis of Flavonoid Glycosides in Rape Bee Pollen Based on Soxhlet-Assisted Matrix Solid Phase Dispersion

A rapid and efficient extraction method based on industrial MCM‐41‐miniaturized matrix solid‐phase dispersion extraction with response surface methodology for simultaneous quantification of six flavonoids in Pollen typhae by ultra‐high‐performance liquid chromatography

A Review on the Recent Progress in Matrix Solid Phase Dispersion

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