2016
DOI: 10.1016/j.jallcom.2016.07.187
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Non-hydrolytic sol-gel processing of chloride precursors loaded at forsterite stoichiometry

Abstract: This paper for the first time investigates the sol-gel reaction of magnesium chloride and silicon tetrachloride, directed at the forsterite (Mg2SiO4) stoichiometry, using dry ethanol and glacial acetic acid as the solvent and chelating agent, respectively. The synthesized particles before and after calcination were characterized by transmission electron microscopy equipped with energy-dispersive X-ray spectroscopy mapping, X-ray diffraction and Fourier transform infrared spectroscopy. According to the results,… Show more

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Cited by 9 publications
(1 citation statement)
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“…In order to overcome this problem, the ball milling technique is adopted to reduce particle size that affects the homogeneity and induces lattice strain in the ceramic materials . In contrast, wet chemical routes such as sol‐gel, hydrothermal, co‐precipitation and combustion methods emerged as potential techniques to achieve the high purity multi‐component oxides with better homogeneity, stoichiometric control and low phase formation temperature . Among the various methods, combustion method is extensively utilised for the preparation of silicate materials due to its cost‐effectiveness, energy efficiency and particles homogeneity …”
Section: Introductionmentioning
confidence: 99%
“…In order to overcome this problem, the ball milling technique is adopted to reduce particle size that affects the homogeneity and induces lattice strain in the ceramic materials . In contrast, wet chemical routes such as sol‐gel, hydrothermal, co‐precipitation and combustion methods emerged as potential techniques to achieve the high purity multi‐component oxides with better homogeneity, stoichiometric control and low phase formation temperature . Among the various methods, combustion method is extensively utilised for the preparation of silicate materials due to its cost‐effectiveness, energy efficiency and particles homogeneity …”
Section: Introductionmentioning
confidence: 99%