Mössbauer spectra and structures of Fe/Fe-N multilayered films formed by Fe sputtering and ECR nitrogen plasma exposure

The stoichiometric iron nitrides γ′‐Fe4N, ε‐Fe3N and ζ‐Fe2N were characterized by Mössbauer spectroscopy. The thermal decomposition of ε‐Fe3N was studied in‐situ by means of a specially developed Mössbauer furnace. We found ε‐Fe3N to γ′‐Fe4N and ε‐Fe3Nx (x ≥ 1.3) as decomposition products and determined the border of γ′/ε transformation at T ≅ 930 K. Mössbauer spectroscopy was applied to study in‐situ the thermal decomposition of the nitridometalate Li3[FeIIIN2] and the formation of Li2[(Li1‐xFeIx)N], the compound with the largest local magnetic field ever observed in an iron containing material. The kinetics of formation and the stability of Li2[(Li1‐xFeIx)N] was of particular interest in the present study.

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In situ — High Temperature Mössbauer Spectroscopy of Iron Nitrides and Nitridoferrates

Ksenofontov

Reiman

Waldeck

et al. 2003

Zeitschrift anorg allge chemie

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Applications of conversion electron Mössbauer spectrometry (CEMS)

Nomura

Ujihira

Vértes

1996

Journal of Radioanalytical and Nuclear Chemistry, Articles

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Nitride formation in iron-cobalt sputtered thin films

1996

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Mössbauer spectra and structures of Fe/Fe-N multilayered films formed by Fe sputtering and ECR nitrogen plasma exposure

Cited by 7 publications

References 27 publications

In situ — High Temperature Mössbauer Spectroscopy of Iron Nitrides and Nitridoferrates

In situ — High Temperature Mössbauer Spectroscopy of Iron Nitrides and Nitridoferrates

Applications of conversion electron Mössbauer spectrometry (CEMS)

Nitride formation in iron-cobalt sputtered thin films

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