2018
DOI: 10.1007/s11030-018-9814-7
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Microwave-assisted green synthesis of 4,5-dihydro-1H-pyrazole-1-carbothioamides in water

Abstract: Rapid, efficient, simple and green procedure for the synthesis of 4,5-dihydro-1H-pyrazole-1-carbothioamides via the multicomponent reaction of aryl aldehydes, acetophenones and thiosemicarbazide in water in the presence of tetrabutylammonium hydroxide under microwave irradiation is reported.

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Cited by 5 publications
(2 citation statements)
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“…Hamid Reza Farmani et al [52] synthesize green protocol is microwave-assisted synthesis of 4, 5-dihydro-1H-pyrazole-1- Jaimin D. Bhatt et al [53] synthesize novel pyrazole clubbed polyhydroquinolines (32) Valentina Molteni et al [54] give microwave assisted one-pot synthesis of pyrazoles (33) in aqueous medium. They perform three synthesis out of which one is pyrazole which is prepared by smith process vial, the 1, 3-diketone and dimethylformamide dimethyl acetal (DMF-DMA) were mixed and the substituted hydrazine monochloride was added followed by addition of distilled H 2 O and AcOH.…”
Section: Mw Assisted Synthesismentioning
confidence: 99%
See 1 more Smart Citation
“…Hamid Reza Farmani et al [52] synthesize green protocol is microwave-assisted synthesis of 4, 5-dihydro-1H-pyrazole-1- Jaimin D. Bhatt et al [53] synthesize novel pyrazole clubbed polyhydroquinolines (32) Valentina Molteni et al [54] give microwave assisted one-pot synthesis of pyrazoles (33) in aqueous medium. They perform three synthesis out of which one is pyrazole which is prepared by smith process vial, the 1, 3-diketone and dimethylformamide dimethyl acetal (DMF-DMA) were mixed and the substituted hydrazine monochloride was added followed by addition of distilled H 2 O and AcOH.…”
Section: Mw Assisted Synthesismentioning
confidence: 99%
“…Hamid Reza Farmani et al [52] . synthesize green protocol is microwave‐assisted synthesis of 4, 5‐dihydro‐1H‐pyrazole‐1‐carbothioamides (31) in water.…”
Section: All Green Approaches For Pyrazole Synthesismentioning
confidence: 99%