Metal organic framework based carbon porous as an efficient dispersive solid phase extraction adsorbent for analysis of methamphetamine from urine matrix

Taghvimi, Arezou; Tabrizi, Ahad Bavili; Dastmalchi, Siavoush; Javadzadeh, Yousef

doi:10.1016/j.jchromb.2019.02.005

Cited by 29 publications

(18 citation statements)

References 50 publications

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“…Their most notable properties, including high specific surface area, porosity easily tuneable by linker choice and the fact that they are readily modifiable, brought significant attention towards a wide spectrum of industrial and scientific applications. They have already found use in catalysis, drug delivery and energy storage, as well as separation techniques [ 62 , 63 , 64 ].…”

Section: Sorbents Based On Metallic Organic Frameworkmentioning

confidence: 99%

Recent Materials Developed for Dispersive Solid Phase Extraction

Ścigalski¹,

Kosobucki²

2020

Molecules

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Solid phase extraction (SPE) is an analytical procedure developed with the purpose of separating a target analyte from a complex sample matrix prior to quantitative or qualitative determination. The purpose of such treatment is twofold: elimination of matrix constituents that could interfere with the detection process or even damage analytical equipment as well as enriching the analyte in the sample so that it is readily available for detection. Dispersive solid phase extraction (dSPE) is a recent development of the standard SPE technique that is attracting growing attention due to its remarkable simplicity, short extraction time and low requirement for solvent expenditure, accompanied by high effectiveness and wide applicability. This review aims to thoroughly survey recently conducted analytical studies focusing on methods utilizing novel, interesting nanomaterials as dSPE sorbents, as well as known materials that have been only recently successfully applied in dSPE techniques, and evaluate their performance and suitability based on comparison with previously reported analytical procedures.

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Section: Sorbents Based On Metallic Organic Frameworkmentioning

confidence: 99%

Recent Materials Developed for Dispersive Solid Phase Extraction

Ścigalski¹,

Kosobucki²

2020

Molecules

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“…Methamphetamine, further, leads to mental and physical disorders in the subjects [4,5]. Therefore, the introduction of novel analytical methods to discriminate methamphetamine is of great importance [6,7]. Several sample preparation methods are applied in complex biological media due to complicated matrix and deficient dosages of the analytes in them.…”

Section: Accepted Manuscriptmentioning

confidence: 99%

“…Probable frangibility, clogging risk of the SPE cartridges, and solvent peculation through solid-phase particles are SPE disadvantages [9]. In order to cover the mentioned problems, the dispersive solid-phase extraction (DSPE) method is selected due to the advantages of high extraction efficiency, lower desorption organic solvents, and favorable preconcentration factor [7]. There are different methods that have been applied for methamphetamine extraction and determination of methamphetamine from urine samples.…”

Section: Accepted Manuscriptmentioning

confidence: 99%

Application of Carbonic Nanosheets Based on Urea Precursors as Dispersive Solid Phase Extraction Adsorbent for Extraction of Methamphetamine from Urine Samples

2020

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“…LC is a more highly developed technique for amphetamines and related metabolites determination [7,9]. DSPE has been applied in sample preparation of various ranges of environmental and biological analytes [18]. Fluorescence and chemiluminescence are established procedures for methamphetamine determination by quantum dots [11].…”

Section: Introductionmentioning

confidence: 99%

“…Recently, dispersive SPE (DSPE) has been introduced as an efficient SPE-based method with the contrast of dispersing of solid phase material in the matrix providing well-interaction of analyte with adsorptive material and enhansing the extraction efficiency. DSPE has been applied in sample preparation of various ranges of environmental and biological analytes [18]. Graphene oxide (GO) presents superior physicochemical properties and cost effective synthesis process [19].…”

Section: Introductionmentioning

confidence: 99%

Dispersive solid‐phase extraction adsorbent of methamphetamine using in‐situ synthesized carbon‐based conductive polypyrrole nanocomposite: focus on clinical applications in human urine

Jabbari

Taghvimi

Dastmalchi

et al. 2019

J of Separation Science

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Arezou Taghvimi contributed equally to this work.Determination of methamphetamine is of great importance in clinical and forensic laboratories because there are low dosages of drugs in the biological media and social problems created due to the methamphetamine consumption. Polymeric carbon based-nano composites are reasonable candidates for dispersive solid phase extraction method due to facial and affordable synthesis process and high selectivity and sensitivity. Nano graphene oxide polypyrolle composite was synthesized and employed as dispersive solid-phase extraction adsorbent for methamphetamine extraction from complex urine matrix. Full characterization of the prepared nano graphene oxide polypyrolle composite was completed and the influential extraction parameters were investigated through one-parameter-at-a-time method. High-performance liquid chromatography detectors were applied as detection and quantification instrument. The optimized extraction parameters included 300 μL of methanol, 10 min of extraction and desorption time, 6000 stirring rate, urine pH value of 10, 60 mg of adsorbent, and 6 mL of urine volume. After outlining the calibration curve, the linear range of the method was considered as 30-800 ng/mL. The detection limit for the suggested method was 9 ng/mL. The analysis of addicted subjects with the proposed method confirmed the utility of the method in different analytical and clinical laboratories. K E Y W O R D Sdispersive solid-phase extraction, graphene oxide, methamphetamine, polypyrrole, urine 606 How to cite this article: Jabbari NR, Taghvimi A, Dastmalchi S, Javadzadeh Y. Dispersive solid-phase extraction adsorbent of methamphetamine using insitu synthesized carbon-based conductive polypyrrole nanocomposite: focus on clinical applications in human urine. J Sep Sci 2020;43:606-613. https://doi.

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Metal organic framework based carbon porous as an efficient dispersive solid phase extraction adsorbent for analysis of methamphetamine from urine matrix

Cited by 29 publications

References 50 publications

Recent Materials Developed for Dispersive Solid Phase Extraction

Recent Materials Developed for Dispersive Solid Phase Extraction

Application of Carbonic Nanosheets Based on Urea Precursors as Dispersive Solid Phase Extraction Adsorbent for Extraction of Methamphetamine from Urine Samples

Dispersive solid‐phase extraction adsorbent of methamphetamine using in‐situ synthesized carbon‐based conductive polypyrrole nanocomposite: focus on clinical applications in human urine

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