Liquid chromatographic analysis of antibacterial drug residues in food products of animal origin

Shaikh, Badar; Moats, W. A.

doi:10.1016/0021-9673(93)80573-q

Cited by 63 publications

(19 citation statements)

References 52 publications

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“…Several articles and reviews describe the analysis of the selected compounds by HPLC-UV and LC-MS from pharmacokinetic studies or determination of drug residues in food products [19][20][21][22][23]. Recently several methods have been developed for the simultaneous determination of pharmaceuticals in the aqueous environment using solid-phase extraction (SPE) and detection by liquid chromatography-tandem mass spectrometry [24][25][26].…”

Section: Introductionmentioning

confidence: 99%

Analysis of antibiotics in urine and wipe samples from environmental and biological monitoring—Comparison of HPLC with UV-, single MS- and tandem MS-detection

Tuerk

Reinders

Dreyer

et al. 2006

Journal of Chromatography B

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Section: Introductionmentioning

confidence: 99%

Analysis of antibiotics in urine and wipe samples from environmental and biological monitoring—Comparison of HPLC with UV-, single MS- and tandem MS-detection

Tuerk

Reinders

Dreyer

et al. 2006

Journal of Chromatography B

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“…They are unstable in acid, and are typically extracted from alkalinised matrices [290]. Both classes of compound have been extracted using MeOH, aqueous buffer, ACN, or mixtures of ACN and aqueous buffer [291]. A number of sample preparation methods for the isolation of macrolides in food matrices have been reported, as described by Wang in a comprehensive review on analysis of macrolides in samples of food, biological and environmental origin [292].…”

Section: Macrolides and Lincosamidesmentioning

confidence: 99%

Current trends in sample preparation for growth promoter and veterinary drug residue analysis

Kinsella

O’Mahony

Malone

et al. 2009

Journal of Chromatography A

181

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A comprehensive review is presented on the current trends in sample preparation for isolation of veterinary drugs and growth promotors from foods. The objective of the review is to firstly give an overview of the sample preparation techniques that are applied in field. The review will focus on new techniques and technologies, which improve efficiency and coverage of residues. The underlying theme to the paper is the developments that have been made in multi-residue methods and particularly multi-class methods for residues of licensed animal health products, which have been developed in the last couple of years. The role of multi-class methods is discussed and how they can be accommodated in future residue surveillance.

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“…in food products of animal origin such as meat and milk. The review covers clean-up procedures, such as, ultrafiltration, liquid -liquid partition, solid-phase extraction, immunoaffinity, and matrix solid-phase dispersion, for use as extraction, deproteinization, and concentration steps [13].…”

Section: Introductionmentioning

confidence: 99%

Multi‐residue methods for confirmatory determination of antibiotics in milk

Samanidou¹,

Nisyriou²

2008

J of Separation Science

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The prevalent use of antibiotics, e. g. sulphonamides, tetracyclines, beta-lactams, macrolides, aminoglycosides, etc., in dairy farming to prevent and treat microbial infections e. g. mastitis, can be a potential source of veterinary drug residues in milk. Antibiotic residues constitute a risk to human health, since they can cause allergic reactions in hypersensitive individuals or they may lead to the appearance of drug-resistant bacteria. Analysis of these residues plays a key role in ensuring food safety. Regulatory agencies in the European Union and in other countries have established maximum residue limits and requirements concerning the performance of analytical methods and the interpretation of the results. This review describes the state of the art in the analytical strategies concerning the multi-class as well as the multi-residue analysis of antibiotics in milk. Since milk is a complex matrix due to its high protein and fat content, which often interfere in analytical procedures, special focus has been placed on sample preparation: extraction and clean-up. Confirmation of antibiotic residues according to European Decision 657/2002/EC has been also discussed.

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Liquid chromatographic analysis of antibacterial drug residues in food products of animal origin

Cited by 63 publications

References 52 publications

Analysis of antibiotics in urine and wipe samples from environmental and biological monitoring—Comparison of HPLC with UV-, single MS- and tandem MS-detection

Analysis of antibiotics in urine and wipe samples from environmental and biological monitoring—Comparison of HPLC with UV-, single MS- and tandem MS-detection

Current trends in sample preparation for growth promoter and veterinary drug residue analysis

Multi‐residue methods for confirmatory determination of antibiotics in milk

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