1998
DOI: 10.1021/jo9718657
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Improved Methods for the Synthesis of [ω-11C]Palmitic Acid

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Cited by 46 publications
(29 citation statements)
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References 11 publications
(36 reference statements)
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“…The symmetrical 4,4 0 -diiododiphenyliodonium salts 2, 3 and 5 were used as precursors for radiofluorinations with The summary clearly shows the important influence of temperature and solvent on the radiochemical yield, showing a maximum at 1408C with DMF as the solvent (runs [4][5][6][7]10,13). This finding agrees with the results obtained by Gail et al 16 since high reaction temperatures seem to be essential for an efficient thermal decomposition of diaryliodonium salts in a highly polar aprotic solvent.…”
Section: Synthesis Of 4-[ 18 F]fluoroiodobenzenementioning
confidence: 99%
“…The symmetrical 4,4 0 -diiododiphenyliodonium salts 2, 3 and 5 were used as precursors for radiofluorinations with The summary clearly shows the important influence of temperature and solvent on the radiochemical yield, showing a maximum at 1408C with DMF as the solvent (runs [4][5][6][7]10,13). This finding agrees with the results obtained by Gail et al 16 since high reaction temperatures seem to be essential for an efficient thermal decomposition of diaryliodonium salts in a highly polar aprotic solvent.…”
Section: Synthesis Of 4-[ 18 F]fluoroiodobenzenementioning
confidence: 99%
“…After allowance for decay, an 83% yield of [C-11]-iodomethane was obtained after 7 min. This process has been successfully applied 22 …”
Section: Preparation and Application Of [C-11]-methylating Agentsmentioning
confidence: 97%
“…Moreover, the Suzuki reaction has already proved to be a reliable and robust synthetic method in the synthesis of several 11 C-labelled compounds. 10,11 In this report, we describe the synthesis of various …”
Section: Introductionmentioning
confidence: 99%