2014
DOI: 10.1016/j.msec.2014.05.079
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Hydrothermal synthesis and thermal evolution of carbonate-fluorhydroxyapatite scaffold from cuttlefish bones

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Cited by 32 publications
(21 citation statements)
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“…The successful transformation of the aragonite from the cuttlefish bone to hydroxyapatite is indicated by characteristic phosphate ( PO43) bands at 1086, 1025, 960, 609, and 562 cm −1 and hydroxyl (–OH) group founded at 3571 and 630 cm −1 (Figure ). Hydrothermal conversion has also resulted in non‐stoichiometric carbonated hydroxyapatite indicated by specific doublet of carbonate group ( CO32) at 1457–1412 cm −1 and carbonate band at 879–872 cm −1 . Mentioned absorption bands of hydroxyapatite are also present in different HA/PCL/PLA scaffolds along with bands associated with polymer phase.…”
Section: Resultsmentioning
confidence: 99%
“…The successful transformation of the aragonite from the cuttlefish bone to hydroxyapatite is indicated by characteristic phosphate ( PO43) bands at 1086, 1025, 960, 609, and 562 cm −1 and hydroxyl (–OH) group founded at 3571 and 630 cm −1 (Figure ). Hydrothermal conversion has also resulted in non‐stoichiometric carbonated hydroxyapatite indicated by specific doublet of carbonate group ( CO32) at 1457–1412 cm −1 and carbonate band at 879–872 cm −1 . Mentioned absorption bands of hydroxyapatite are also present in different HA/PCL/PLA scaffolds along with bands associated with polymer phase.…”
Section: Resultsmentioning
confidence: 99%
“…Synthetic nanocrystalline apatites represent a model for the basic constituent of the inorganic part of bones (65)(66)(67)(68)(69)(70)(71)(72)(73)(74)(75) wt.%, depending on age and sex) [11], with a general formula [34] Ca 10−x (PO 4 ) 6−x (HPO 4 or CO 3 ) x (OH) 2−x with 0 ≤ x ≤ 2. These nanocrystals exhibit in particular special surface features as shown in previous investigations using spectroscopic techniques [35][36][37][38][39][40]: precipitated nanocrystals possess a prominent structured hydrated layer on their surfaces, which is gradually converted into more stable apatite domains during aging.…”
mentioning
confidence: 99%
“…The carbonates are also revealed at 880-1417 cm -1 [13]. Figure 4 shows the XRD pattern of the investigated glass samples containing raw materials.…”
Section: Resultsmentioning
confidence: 97%