Dyeing Chitin/Cellulose Composite Fibers with an Acid Dye

Shimizu, Yoshiaki; Nakajima, Tetsuo; Yoshikawa, Masayuki; Takagishi, Toru

doi:10.1177/004051750207200701

Cited by 20 publications

(28 citation statements)

References 6 publications

(4 reference statements)

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“…The dry intensity of the blend filaments containing 2.89% and 6.46% (w/w) chitin content is 1.98 and 1.92 cN Â dtex À1 , respectively, which is much higher than that of Crabyon, i.e., 0.7 cN Â dtex À1 . 15 Therefore, the cellulose/chitin filament we prepared has improved intensity.…”

Section: Degree Of Orientation and Mechanical Propertiesmentioning

confidence: 98%

“…The blend solution was filtered for the first time which was defined as IF filtration, deaerated under 0.08 Mpa vacuum for 15 h, and aging at [15][16][17][18][19][20][21][22][23][24][25][26] C for 10 h until a certain aging extent was reached. Then the spinning solution was filtered for the second time, which was defined as IIF filtration.…”

Section: Spinning Conditionmentioning

confidence: 99%

“…But the mechanical property of Crabyon V R is only 0.7 cN Â dtex À1 . 14,15 And there is no any report concerned with the production of filament prepared from chitin-cellulose xanthate blend solution because of more difficulty in filament production.…”

Section: Introductionmentioning

confidence: 99%

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The preparation and properties of cellulose/chitin blend filaments

Sun

2009

J of Applied Polymer Sci

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The focus of this article is the preparation and characterization of cellulose/chitin blend filaments obtained from cellulose/chitin xanthate blend solution over the experimental blend ratio, i.e., 2.89% and 6.46% (w/w) chitin content. The addition of chitin xanthate into cellulose xanthate leads to an increase of intermittence rate and the blend solution has good filtering property. Scanning electronic microscope photos shows that there exist grooves on the filaments surface, which are becoming coarse with increasing chitin content. The mechanical properties of the spun blend filaments is much higher than that of CrabyonV R fiber, which proves that the viscose method we adopt here is an efficient way to prepare cellulose/chitin blend filaments with satisfactory mechanical properties and processing property. Based on the data from X-ray, sonic velocity, equilibrium regain rate, and accessibility, it is concluded that the degree of crystallinity, modulus, degree of orientation, density, equilibrium regain rate, and accessibility of blend filaments decreases with increasing chitin content in the blend filaments in the experiment scope.

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Section: Degree Of Orientation and Mechanical Propertiesmentioning

confidence: 98%

Section: Spinning Conditionmentioning

confidence: 99%

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The preparation and properties of cellulose/chitin blend filaments

Sun

2009

J of Applied Polymer Sci

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“…이 이외에도 폴리에스터 나 나일론과 같은 합성섬유에 키토산으로 가공한 후 오배자의 염색 특성을 고찰한 선행 연구 등도 있다 (Hong et al, 2005a, b, c, d). (Shimizu et al, 2004;Shimizu et al, 2002 (Noh & Lee, 2014;Shin et al, 2005). …”

Section: 오배자 염색에 관한 선행연구로는 대두섬유에 있어 오배자unclassified

Gallnut dyeing of Crabyon Fiber Contained Cotton Towels

Woo¹,

Lee²

2015

Fashion & Textile Research Journal

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: The purpose of this study is to investigate the dyeability of crabyon fiber contained cotton towels after dyeing with gallut. In this study, the colorants of gallnut were extracted with boiling water at 60 o C and 60min. Crabyon, composite fiber of Chitin/Chitosan and cellulose, is manufactured by uniformly blending Chitin/Chitosan and cellulose viscose and extruding the blended viscose into spin-bath. Cotton towels with crabyon fiber dyed with extracted solution from gallnut according to concentration, temperature and time. Crabyon fiber contained cotton towels dyed using gallnut were pre of post-mordanted using Al, Cu, and Fe. The dyeability(K/S) and color characteristics(L * , a * , b * , C, and h(color angle)) of dyed crabyon fiber contained cotton towels were measured by computer color matching machine and photographs. The crabyon fiber composition of cotton towels was conformed by amide peak(-CONH-) of chitin or chitosan of FT-IR spectroscopy. The results obtained were as follows; The amide peak of crabyon fiber contained cotton towels appeared at about 1652 cm -1. The dyeability of crabyon fiber contained cotton towel was increased gradually with increasing concentration of gallnut dyeing solution and saturated at about 150%(o.w.f). The optimum dyeing temperature and dyeing time were 90~100 o C and 80minutes expectively. The crabyon fiber contained cotton towels were dyed reddish yellow by non, Al, and Cu mordanting, reddish blue by Fe mordanting, respectively. The fastness to washing according to concentration of gallnut in and mordanting method indicated good grade result as more than 3~4 degree in all conditions.

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“…However, among the relevant studies, the effects of different degrees of deacetylation of chitosan on the adsorption of specific dyes, or the formula of using fixed chitosan materials for the adsorption of a single dye have not been investigated [13]- [15]. Moreover, there are very little studies focusing on the different forms of chitosan materials or the adsorptive properties of different types of dyes.…”

Section: Introductionmentioning

confidence: 99%

Comparison of Dye Adsorption of Three Forms of Chitosan

Lin¹,

Chang²,

Chang³

et al. 2014

ACES

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The purpose of this project is to explore the adsorption rates of different dye methods (direct, reactive, acidic, disperse, azo dyes) in three shapes of chitosan materials (film, microsphere, and scaffold) which were formed by 88% deacetylation degree of chitosan. Results of this research suggest that the samples with larger specific surface areas tend to have shorter adsorption times. Among the three samples, the chitosan scaffold reached the adsorptive saturation on the third day, showing the shortest adsorption time of the direct, reactive, acidic, dispersive and azo dyes, whereas the chitosan film reached the adsorptive saturation on the eighth day, giving it the longest adsorption time of the dyes.

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Dyeing Chitin/Cellulose Composite Fibers with an Acid Dye

Cited by 20 publications

References 6 publications

The preparation and properties of cellulose/chitin blend filaments

The preparation and properties of cellulose/chitin blend filaments

Gallnut dyeing of Crabyon Fiber Contained Cotton Towels

Comparison of Dye Adsorption of Three Forms of Chitosan

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