Development of a process for obtaining non-mutagenic madder root (Rubia tinctorum) extract for textile dyeing

Derksen, G.C.H.; Holthoon, Frédérique L. van; Willemen, Hendra M.; Krul, Cyrille; Franssen, M.C.R.; Beek, T.A. van

doi:10.1016/j.indcrop.2021.113344

Cited by 13 publications

(8 citation statements)

References 56 publications

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“…However, in recent times for various reasons there is a renewed interest in natural dyes. To facilitate the re-introduction of natural dyes, over the last 25 years many papers have appeared, for instance on screening methods for agronomic studies of dye plants [2,3], the fastness of dyed textiles [4], the colorimetric properties of dye plants and their individual constituents [5], mild extraction methods for textiles [6][7][8], degradation of dyes [9][10][11], safety of natural dyes [12], the development of new production routes [13], and analysis of dyed textiles [1,14]. Concerning the latter topic, natural dye analysis is of great importance for historians and conservators.…”

Section: Introductionmentioning

confidence: 99%

Microextraction of Reseda luteola-Dyed Wool and Qualitative Analysis of Its Flavones by UHPLC-UV, NMR and MS

et al. 2021

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Detailed knowledge on natural dyes is important for agronomy and quality control as well as the fastness, stability, and analysis of dyed textiles. Weld (Reseda luteola L.), which is a source of flavone-based yellow dye, is the focus of this study. One aim was to reduce the required amount of dyed textile to ≤50 μg for a successful chromatographic analysis. The second aim was to unambiguously confirm the identity of all weld flavones. By carrying out the extraction of 50 μg dyed wool with 25 μL of solvent and analysis by reversed-phase UHPLC at 345 nm, reproducible chromatographic fingerprints could be obtained with good signal to noise ratios. Ten baseline separated peaks with relative areas ≥1% were separated in 6 min. Through repeated polyamide column chromatography and prepHPLC, the compounds corresponding with the fingerprint peaks were purified from dried weld. Each was unequivocally identified, including the position and configuration of attached sugars, by means of 1D and 2D NMR and high-resolution MS. Apigenin-4′-O-glucoside and luteolin-4′-O-glucoside were additionally identified as two trace flavones co-eluting with other flavone glucosides, the former for the first time in weld. The microextraction might be extended to other used dye plants, thus reducing the required amount of precious historical textiles.

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Section: Introductionmentioning

confidence: 99%

Microextraction of Reseda luteola-Dyed Wool and Qualitative Analysis of Its Flavones by UHPLC-UV, NMR and MS

et al. 2021

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“…In an experimental design for textile dye extraction from Rubia tinctorum L., Derksen et al heated the plant roots in the refluxing ethanol–water (1:1 w / w ) solvent, followed by filtration using reduced pressure. As a result of chromatographic analysis, alizarin was found in the dye extract 71 . Moreover, Zhu et al extracted the alizarin component from Morinda officinalis How.…”

Section: Extraction Methods Of Alizarin From Rubiaceae Family Plantsmentioning

confidence: 99%

Alizarin old and new: Extraction techniques for coloration, advances in detection methods for historical textiles and novel applications as a functional dye

Mushtaq²,

Zhao

et al. 2023

Coloration Technology

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The current study provides the first review of alizarin, a natural dye, in terms of its historical aspects and its potential for functional applications in textiles. The review begins with a brief overview of natural alizarin and its occurrence in Rubiaceae family plants, followed by a discussion of alizarin acquisition from its botanical sources through conventional and advanced extraction methods. A special emphasis of this study is on the identification of natural alizarin colourants in archaeological and cultural textiles by using analytical methods based on reflectance, Raman spectroscopy, mass spectrometry and chromatographic profiles. In addition, the functional properties of natural alizarin, including its antimicrobial activity, anti‐oxidant activity, insect repellence and ultraviolet protection, are analysed. This paper summarises the methods for obtaining alizarin for coloration, as well as advanced techniques for detecting alizarin in historical textiles, and potential applications of natural alizarin as a functional textile dye.

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“…The GB and GY dyes were obtained from Wuhan Green Food Biological Engineering Co. Ltd. (China). The chemical structures of the main components of MR 34 , GB 35 , 36 , and GY 37 are shown in Fig. 1 .…”

Section: Methodsmentioning

confidence: 99%

“…Besides, in the dyeing with binary mixtures of dyes, the dye amount removal ratio of each dye from the dyed wool yarn was occasionally different, for example, in Sample 55 in Table 2, shifting the λ max of K/S after soaping. Furthermore, these natural plant dyes contain many compounds [51][52][53][54] , which are also adsorbed in the substance and contribute to the color shade of the dyed sample in its application. Hence, after soaping the wool yarn dyed with a single dye, the color shift was caused by the change in the amount of all the compounds in the wool yarn, although the λ max of K/S was the same.…”

Section: Dyeing Of Wool Yarn With Natural Dye Mixturesmentioning

confidence: 99%

Sustainable fashion: eco-friendly dyeing of wool fiber with novel mixtures of biodegradable natural dyes

Lin

Jiang

Xiao

et al. 2022

Sci Rep

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Natural materials, especially natural colorants, have achieved global prominence and might be regarded as an environmentally beneficial alternative to hazardous synthetic dyes. The color limitation of natural dyes hinders their application in textiles. The present work aims to prepare more color shades of wool yarns via dyeing with ternary natural dye mixtures without adding mordants. In this study, a sustainable dyeing approach for wool yarn was evaluated with three natural dyes, madder red (MR), gardenia blue (GB), and gardenia yellow (GY), by following an industrial dyeing procedure in the absence of a mordant. In the beginning, a preliminary assessment of dye stabilities was carried out, and it was found that the three natural dyes were sensitive to temperature and acid (degradation tendency). Then, the dyeing behavior was systematically evaluated, including a single natural dye, a binary natural dye mixture, and a ternary natural dye mixture. The results of wool yarn dyeing with a single natural dye show that the dye exhaustion percentage (E%) of MR, GY, and GB was in the ranges of 78.7–94.1%, 13.4–44.1%, and 54.8–68.5%, respectively. The dyeing results of wool yarns dyed with binary and ternary natural dye mixtures (a color triangle framework of dyed wool yarn) were characterized by colorimetric values (L*, a*, b*, C*, h, and K/S), and are presented to enlighten various colorful shades. Finally, color uniformity and colorfastness tests confirmed the vital contribution of natural dyes toward wool yarn coloration. Particularly, colorfastness to washing confirmed the stability of natural dyes with reference to the lower amount of dyes released into the effluent, which is beneficial for the environment. Overall, this study provides a good background for enhancing the industrialization trend of natural dyes by modulating their dyeing scheme.

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Development of a process for obtaining non-mutagenic madder root (Rubia tinctorum) extract for textile dyeing

Cited by 13 publications

References 56 publications

Microextraction of Reseda luteola-Dyed Wool and Qualitative Analysis of Its Flavones by UHPLC-UV, NMR and MS

Microextraction of Reseda luteola-Dyed Wool and Qualitative Analysis of Its Flavones by UHPLC-UV, NMR and MS

Alizarin old and new: Extraction techniques for coloration, advances in detection methods for historical textiles and novel applications as a functional dye

Sustainable fashion: eco-friendly dyeing of wool fiber with novel mixtures of biodegradable natural dyes

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