Determination of Trace Elements in Meat and Fish Samples by MIP OES Using Solid-Phase Extraction

Sá, Ivero Pita de; Higuera, Julymar M.; Costa, Vinícius Câmara; Costa, José Arnaldo Santana; Paranhos, Caio Márcio; Nogueira, Ana Rita A.

doi:10.1007/s12161-019-01615-3

Cited by 26 publications

(15 citation statements)

References 39 publications

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“…ICP-OES is by far the most commonly applied technique for the analysis of food samples [ 16 , 18 , 22 , 33 ] because it offers simultaneous multi-element measurement, capabilities for sensitive determination of refractory elements, quantification of nonmetals, and high analytical throughput. Microwave induced plasma optical emission spectrometry (MIP-OES) using the magnetically excited microwave plasma source has also been recently applied to fish and seafood [ 34 , 35 ], mainly because it is characterized by detection limits down to sub-ppb levels, significant cost reduction, and simpler spectra than ICP-OES. However, at present, both ICP-OES and MIP-OES fail to meet the needs required in routine applications when the determination of elements at trace or ultra-trace concentrations is in demand.…”

Section: Analytical and Chemometric Methodologies For Element And mentioning

confidence: 99%

“…Nowadays, the most used and useful digestion technique for a wide range of analytes and sample matrices is the high-pressure digestion using a closed-vessel microwave system [ 15 , 16 , 17 , 18 , 20 , 24 , 34 , 36 , 41 , 49 , 57 ]. This technique increases the sample throughput, minimizes analyte losses during the decomposition, reduces both contamination risk (especially for trace analytes) and consumption of reagents, and is more effective, resulting in low residual carbon content of digested samples [ 57 ].…”

Section: Analytical and Chemometric Methodologies For Element And mentioning

confidence: 99%

“…In addition to high-pressure closed-vessel microwave digestion, digestion involving opened vessels or classical dry-ashing digestion is generally performed. In wet-acid digestion, HNO 3 alone [ 15 , 16 , 20 , 24 ] or combined with H 2 O 2 [ 17 , 18 , 28 , 34 , 36 , 41 , 49 ] and, occasionally, HCl [ 35 ] or HClO 4 [ 22 , 23 , 33 ], is the most commonly used reagent. However, several novel approaches or adaptations to established procedures for sample preparation have been recently introduced.…”

Section: Analytical and Chemometric Methodologies For Element And mentioning

confidence: 99%

See 2 more Smart Citations

Advances in Troubleshooting Fish and Seafood Authentication by Inorganic Elemental Composition

Varrà

Ghidini

Husáková

et al. 2021

Foods

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The demand for fish and seafood is growing worldwide. Meanwhile, problems related to the integrity and safety of the fishery sector are increasing, leading legislators, producers, and consumers to search for ways to effectively protect themselves from fraud and health hazards related to fish consumption. What is urgently required now is the availability of reliable, truthful, and reproducible methods assuring the correspondence between the real nature of the product and label declarations accompanying the same product during its market life. The evaluation of the inorganic composition of fish and seafood appears to be one of the most promising strategies to be exploited in the near future to assist routine and official monitoring operations along the supply chain. The present review article focuses on exploring the latest scientific achievements of using the multi-elemental composition of fish and seafood as an imprint of their authenticity and traceability, especially with regards to the geographical origin. The scientific literature of the last 10 years focusing on the analytical determination and statistical elaboration of elemental data (alone or in combination with methodologies targeting other compounds) to verify the identity of fishery products is summarized and discussed.

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Section: Analytical and Chemometric Methodologies For Element And mentioning

confidence: 99%

Section: Analytical and Chemometric Methodologies For Element And mentioning

confidence: 99%

Section: Analytical and Chemometric Methodologies For Element And mentioning

confidence: 99%

See 1 more Smart Citation

Advances in Troubleshooting Fish and Seafood Authentication by Inorganic Elemental Composition

Varrà

Ghidini

Husáková

et al. 2021

Foods

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show abstract

“…They are often used as a chromatographic stationary phase or to selectively extract trace molecules from complex matrices using the solid phase extraction technique. During this process, the analytes are separated and preconcentrated, resulting in a lower limit of detection (LOD) than with classical techniques, even in complex samples [21] such as fish, meat [22,23], or milk [24]. This type of system can also be used for the purification and enantioselective separation of drugs [25,26], for example by forming enantioselective membranes [27].…”

Section: Fundamentals About Mips and Their Adaptation For Nanomedicine 11 Historical Applicationsmentioning

confidence: 99%

Hybrids Molecularly Imprinted Polymers: The Future of Nanomedicine?

Garnier¹,

Sabbah²,

Ménager³

et al. 2021

Preprint

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Molecularly imprinted polymers (MIPs) have been widely used in nanomedicine during the last few years. However, their potential is limited by their intrinsic properties resulting, for instance, in lack of control in drug release processes or complex detection for in vivo imaging. Recent attempts in creating hybrid nanomaterials combining MIPs with inorganic nanomaterials succeeded in providing a wide range of new interesting properties suitable for nanomedicine. Through this review, we aim to illustrate how hybrids molecularly imprinted polymers may improve patient care with enhanced imaging, treatments and combination of both.

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“…[13][14][15] Solid phase extraction (SPE) is a preferred technique due to its merits such as simple operation, higher enrichment factor, and the ability to combine with other detection techniques. [16][17][18][19] However, this procedure suffers from certain shortcomings such as solvent loss, large secondary waste, and a long procedure. 20 In addition, a liquid sample is passed through a column containing an adsorbent in conventional SPE.…”

Section: Introductionmentioning

confidence: 99%

Dispersive Micro-solid Phase Extraction with Fibrous TiO2@g- C3N4 Nanocomposites Coupled with ICP-MS for the Determination of Cobalt and Nickel in Environmental and Biological Samples

Chen¹,

Liu²,

Yan³

et al. 2020

At.Spectrosc.

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In this work, fibrous TiO2@g-C3N4 nanocomposites (FTGCNCs) were used for dispersive micro-solid phase extraction of Co and Ni prior to their determination by inductively coupled plasma mass spectrometry. As a new adsorbent, the surface on FTGCNCs have rich functional groups such as-NH2,-NH-and =N-, which can selectively adsorb target ions. The adsorption behaviors of Co and Ni on FTGCNCs were investigated. The results indicated that the analytes were quantitatively retained on FTGCNCs in the pH range of 5.0-8.0 and eluted completely with 1.0 mL of 0.5 mol L-1 HNO3 solution. The main factors influencing the preconcentration and determination of the analytes were investigated in detail, including the pH of the sample solution, dosage of adsorbent, extraction/elution time, elution parameters and sample volumes. Under the optimum conditions, the detection limits of this method were 0.12 pg mL-1 and 1.34 pg mL-1 for Co and Ni, respectively. The relative standard deviations were 3.9% for Co and 4.8% for Ni (n=9, c=1.0 ng mL-1). This method was used for the determination of trace/ultra-trace Co and Ni in environmental water samples with satisfactory results. In order to verify this method, three certified reference materials of stream sediment, human hair and mussel were analyzed using the proposed method, and the determined results were in agreement with the certified values.

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Determination of Trace Elements in Meat and Fish Samples by MIP OES Using Solid-Phase Extraction

Cited by 26 publications

References 39 publications

Advances in Troubleshooting Fish and Seafood Authentication by Inorganic Elemental Composition

Advances in Troubleshooting Fish and Seafood Authentication by Inorganic Elemental Composition

Hybrids Molecularly Imprinted Polymers: The Future of Nanomedicine?

Dispersive Micro-solid Phase Extraction with Fibrous TiO2@g- C3N4 Nanocomposites Coupled with ICP-MS for the Determination of Cobalt and Nickel in Environmental and Biological Samples

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