The tensile behaviour of single crystals of the unidirectionally-solidified AI-AI3Ni fibrous and AI-CuAI2 lamellar eutectics has been investigated at ambient and elevated temperatures. Fractured specimens have been studied directly by scanning electron microscopy, and longitudinal sections through each fracture surface by optical microscopy. At low temperatures, fracture of the AI-AIzNi eutectic is caused by the brittle failure of AI3Ni fibres. At intermediate temperatures broken fibres may be present without causing composite fracture, whilst at high temperatures fibre pull-out occurs. The properties of the AI-CuAI2 eutectic are controlled by the brittle CuAI2 phase, except when the temperature is such that both phases are plastic. During fracture at high temperature the AI-CuAI2 eutectic undergoes micromorphological degradation in the vicinity of the fracture surface.
q. IntroductionUnidirectionally-solidified eutectics have been studied because their strength coupled with good thermal stability may well give advantages over more conventional materials. The high temperature strength of a number of systems has been measured [1][2][3][4][5] but no work has been done specifically on the fractography of eutectic composites at varying temperatures. Salkind and co-workers [6,7] have studied the tensile properties of aligned polycrystalline A1-AI~Ni fibrous and A1-CuA12 lamellar eutectics up to 773K (500~ They found that the strength of both materials was reduced at elevated temperatures and that the A1-CuAlz eutectic began to show large elongations at temperatures greater than approximately 623K (350~ Crossman et al [8] confirmed these results for the A1-CuA12 eutectic, as did Butcher et al [9] who also observed microstructural coarsening after fracturing at high temperatures. Fractographic techniques have been used to study the room-temperature fracture of aligned polycrystalline A1-A13Ni eutectic in tension [6,7,10] and aligned polycrystalline A1-CuA12 eutectic in tension [6,7,10] and compression [11]. Tidy and Chadwick [12] have used scanning electron microscopy to study fracture surfaces of aligned single crystals of the A1-CuA12 eutectic deformed in bending at various temperatures.The aim of the present work was to study the effect of temperature on the fracture characteristics of aligned single-crystal specimens of the AI-A13Ni eutectic and the A1-CuA12 eutectic. The fracture surfaces were studied by scanning electron microscopy and longitudinal sections were taken through the fracture surfaces and studied by optical microscopy.
Experimental procedureAlloys of eutectic composition were made up from aluminium of 99.998 ~ purity and copper and nickel of 99.999 ~ purity. They were melted under argon in recrystallized alumina crucibles and cast into long flat ingots of rectangular cross-section. These ingots were placed singly in graphite moulds, enclosed in a silica tube, and directionally solidified horizontally under