Characterization of alkyl polyglycosides by both reversed-phase and normal-phase modes of high-performance liquid chromatography

Czichocki, G.; Fiedler, Harald; Haage, K.; Much, Helmut; Weidner, Steffen M.

doi:10.1016/s0021-9673(01)01459-5

Cited by 24 publications

(11 citation statements)

References 27 publications

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“…Analysis of food constituents by MALDI-MS has been discussed in a review (Careri, Bianchi, & Corradini, 2002) and Czichocki et al (2002) have discussed the convenience of MALDI for monitoring HPLC-separated alkyl polyglucosides used as sugar surfactants. DHB has proved to be the best matrix for detection of starch hydrolysate used to adulterate fruit juices (Zídková & Chmelík, 2001).…”

Section: A Food Industrymentioning

confidence: 99%

Analysis of carbohydrates and glycoconjugates by matrix‐assisted laser desorption/ionization mass spectrometry: An update covering the period 2001–2002

Harvey¹

2008

Mass Spectrometry Reviews

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This review is the second update of the original review on the application of MALDI mass spectrometry to the analysis of carbohydrates and glycoconjugates that was published in 1999. It covers fundamental aspects of the technique as applied to carbohydrates, fragmentation of carbohydrates, studies of specific carbohydrate types such as those from plant cell walls and those attached to proteins and lipids, studies of glycosyl-transferases and glycosidases, and studies where MALDI has been used to monitor products of chemical synthesis. Use of the technique shows a steady annual increase at the expense of older techniques such as FAB. There is an increasing emphasis on its use for examination of biological systems rather than on studies of fundamental aspects and method development and this is reflected by much of the work on applications appearing in tabular form.

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Section: A Food Industrymentioning

confidence: 99%

Analysis of carbohydrates and glycoconjugates by matrix‐assisted laser desorption/ionization mass spectrometry: An update covering the period 2001–2002

Harvey¹

2008

Mass Spectrometry Reviews

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“…Although analysis can be performed below 200 nm, there is no paper describing the analysis of APGs in such conditions. The use of a refractive index detector (Qin et al 2006) and evaporative light scattering detector (ELSD) (Elfakir and Lafosse 1997;Chaimbault et al 1999;Czichocki et al 2002) has been reported. However, sensitivity of a refractive index detector is low and its usage is limited to the control of APG synthesis or biodegradation studies.…”

Section: Introductionmentioning

confidence: 99%

“…Similarly, the use of ELSD has been reported only in papers describing the control of APG synthesis or the chromatographic separation of APGs. Moreover, the analytical signal of particular APG homologues being analysed by ELSD is different (Czichocki et al 2002). Here, liquid chromatography with mass spectrometric detection (HPLC-MS) was found to be a good alternative (Eichhorn and Knepper 1999;Kuhn and Neumbert 2004).…”

Section: Introductionmentioning

confidence: 99%

Investigations on the biodegradation of alkylpolyglucosides by means of liquid chromatography–electrospray mass spectrometry

et al. 2007

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The biodegradation of alkylpolyglucosides (APGs) was studied under the conditions of the OECD Screening Test with activated sludge as an inoculum. An influence of alkyl and sugar chain length on the biodegradation rate and a central scission pathway of the biodegradation were investigated. The liquid chromatography-electrospray mass spectrometry technique was used for alkylpolyglucoside analysis and for identification and semiquantitative determination of metabolites. It was found that APGs with a longer alkyl chain were biodegraded faster than those with a shorter one. However, a longer sugar chain caused slower biodegradation of APGs. The central scission pathway of biodegradation was also confirmed.

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“…Detailed measurements such as high-performance liquid chromatography (HPLC) (6)(7)(8) provide substantially more information on the components. Using reversed-phase isocratic or gradient HPLC, APGs are separated according to their alkyl chain length.…”

Section: Introductionmentioning

confidence: 99%

Characterization of Mixtures of Alkyl Polyglycosides (Plantacare) by Liquid Chromatography-Electrospray Ionization Quadrupole Time-of-Flight Mass Spectrometry

Kühn

Neubert

2004

Pharm Res

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Characterization of alkyl polyglycosides by both reversed-phase and normal-phase modes of high-performance liquid chromatography

Cited by 24 publications

References 27 publications

Analysis of carbohydrates and glycoconjugates by matrix‐assisted laser desorption/ionization mass spectrometry: An update covering the period 2001–2002

Analysis of carbohydrates and glycoconjugates by matrix‐assisted laser desorption/ionization mass spectrometry: An update covering the period 2001–2002

Investigations on the biodegradation of alkylpolyglucosides by means of liquid chromatography–electrospray mass spectrometry

Characterization of Mixtures of Alkyl Polyglycosides (Plantacare) by Liquid Chromatography-Electrospray Ionization Quadrupole Time-of-Flight Mass Spectrometry

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