Application of Graphene-based Solid-Phase Extraction Coupled with Ultra High-performance Liquid Chromatography-Tandem Mass Spectrometry for Determination of Macrolides in Fish Tissues

Wu, Jianbing; Qian, Yongsheng; Zhang, Chuanlan; Zheng, Tinglu; Chen, Linyao; Lu, Yanbin; Wang, Huizhong

doi:10.1007/s12161-013-9563-2

Cited by 24 publications

(9 citation statements)

References 37 publications

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“…The developed SPE-GO-MPPS isolated metal ions from complex matrices with less interference. Excellent sensitivity (145)(146)(147)(148)(149)(150)(151)(152)(153)(154)(155)(156)(157)(158)(159)(160)(161)(162) ng L -1 ), great enrichment factor (325), and good recovery (99-103%) were obtained. Selectivity was considered in the presence of various coexisting ions with > 90% extraction recovery.…”

Section: Applications Of Graphene-based Spe In Biological Sample Analmentioning

confidence: 94%

Graphene-Based Materials as Solid Phase Extraction Sorbent for Trace Metal Ions, Organic Compounds, and Biological Sample Preparation

Ibrahim

Nodeh

Sanagi

2015

Critical Reviews in Analytical Chemistry

111

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Graphene is a new carbon-based material that is of interest in separation science. Graphene has extraordinary properties including nano size, high surface area, thermal and chemical stability, and excellent adsorption affinity to pollutants. Its adsorption mechanisms are through non-covalent interactions (π-π stacking, electrostatic interactions, and H-bonding) for organic compounds and covalent interactions for metal ions. These properties have led to graphene-based material becoming a desirable adsorbent in a popular sample preparation technique known as solid phase extraction (SPE). Numerous studies have been published on graphene applications in recent years, but few review papers have focused on its applications in analytical chemistry. This article focuses on recent preconcentration of trace elements, organic compounds, and biological species using SPE-based graphene, graphene oxide, and their modified forms. Solid phase microextraction and micro SPE (µSPE) methods based on graphene are discussed.

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Section: Applications Of Graphene-based Spe In Biological Sample Analmentioning

confidence: 94%

Graphene-Based Materials as Solid Phase Extraction Sorbent for Trace Metal Ions, Organic Compounds, and Biological Sample Preparation

Ibrahim

Nodeh

Sanagi

2015

Critical Reviews in Analytical Chemistry

111

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“…Regarding the mass spectrometry conditions, the selection of the precursor and product ion was first carried out by direct infusion of As a common additive reagent, formic acid is often included in the mobile phase to provide protons and yield improved ionization efficiency. 20 The results revealed that 0.1% formic acid will increase the MS response and improve the peak shape, while a formic acid content that is too high has no obvious effect. Consequently, ACN containing 0.1% formic acid was used as the optimal organic phase.…”

Section: Chromatography and Mass Spectrometrymentioning

confidence: 94%

Development and validation of an LC‐MS/MS method for quantifying nine antimicrobials in human serum and its application to study the exposure of Chinese pregnant women to antimicrobials

Yue

Pan³

et al. 2020

Clinical Laboratory Analysis

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“…On basis of the characteristics of alkalescence and lipophilic molecules, various solvents were applied to the extraction of macrolide compounds. The common solvents such as methanol (Wu et al, 2013), acetonitrile (Błądek, Posyniak, Gajda, Gbylik, & Żmudzki, 2012), Tris buffer (Dubois, Fluchard, Sior, & Delahaut, 2001), phosphate buffer solution (García-Mayor, Garcinuño, Fernández-Hernando, & Durand-Alegría, 2006) or ethyl acetate (Wang et al, 2014) were reported. In this study, the extraction efficiency of three extraction solvents including methanol, acetonitrile and ethyl acetate was compared.…”

Section: Extractionmentioning

confidence: 99%

Molecularly imprinted solid-phase extraction for the determination of ten macrolide drugs residues in animal muscles by liquid chromatography–tandem mass spectrometry

et al. 2016

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A simple and sensitive method based on molecularly imprinted solid-phase extraction coupled with liquid chromatography-tandem mass spectrometry was developed for the determination of the residues of ten macrolide drugs in swine, cattle and chicken muscles samples. The molecularly imprinted polymers (MIPs) were synthesized using tylosin as a template and methacrylic acid as a functional monomer. Samples were extracted with sodium borate buffer solution and ethyl acetate, and purified by the MIP cartridge. The results showed that the cartridge exhibited good recognition performance for macrolides, and better purification effect than the traditional solid-phase extraction cartridges. Recoveries of analytes at three spiking levels 1, 5 and 20μgkg(-1) ranged from 60.7% to 100.3% with the relative standard deviations less than 14%. The limits of detection of the method were between 0.1 and 0.4μgkg(-1). The method is useful for the routine monitoring of the residues of macrolide drugs in animal muscles.

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Application of Graphene-based Solid-Phase Extraction Coupled with Ultra High-performance Liquid Chromatography-Tandem Mass Spectrometry for Determination of Macrolides in Fish Tissues

Cited by 24 publications

References 37 publications

Graphene-Based Materials as Solid Phase Extraction Sorbent for Trace Metal Ions, Organic Compounds, and Biological Sample Preparation

Graphene-Based Materials as Solid Phase Extraction Sorbent for Trace Metal Ions, Organic Compounds, and Biological Sample Preparation

Development and validation of an LC‐MS/MS method for quantifying nine antimicrobials in human serum and its application to study the exposure of Chinese pregnant women to antimicrobials

Molecularly imprinted solid-phase extraction for the determination of ten macrolide drugs residues in animal muscles by liquid chromatography–tandem mass spectrometry

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