“…189 It is important to note, that the related higher energy technique, RBS, provides beneficial complementary here in that it may probe film thicknesses up to B200 nm due to the deeper probing depth compared with ISS. 229 The efficacy of RBS, however, diminishes with smaller overlayer thicknesses (o3 nm) however, and as such ISS is much more suited for applications such as modelling growth modes on the atomic scale.…”
X-ray photoelectron spectroscopy (XPS) has achieved maturity as an analytical technique in that it is a ubiquitous tool in the materials community, however as made apparent by recent reviews highlighting...
“…189 It is important to note, that the related higher energy technique, RBS, provides beneficial complementary here in that it may probe film thicknesses up to B200 nm due to the deeper probing depth compared with ISS. 229 The efficacy of RBS, however, diminishes with smaller overlayer thicknesses (o3 nm) however, and as such ISS is much more suited for applications such as modelling growth modes on the atomic scale.…”
X-ray photoelectron spectroscopy (XPS) has achieved maturity as an analytical technique in that it is a ubiquitous tool in the materials community, however as made apparent by recent reviews highlighting...
“…The composition is found to be stoichiometric in the range of 0·1 ,;;; x ,;;; 0·2. Results given in [5] for nitride layers from SiH 4 and NH 3 show, that with increasing NH 3/SiH4 gas ratio the composition became stoichiometric as an saturation level. With the glow discharge method however it is possible to further increase the N NIN si-ratio.…”
Section: Discussionmentioning
confidence: 99%
“…A detailed description of the analysis technique has been given elsewhere [3]. For convenience themost important features of the analysis are summarized.…”
Section: Discussionmentioning
confidence: 99%
“…Thecomposition of all sampies is homogeneous over the entire layer, the silicon substrate the yield ofbackscattered particles is reduced (channeling effect) and a more accurate determination of the nitrogen concentration can be made. These techniques have been used to analyse silicon dioxide layers [3] and nitride layers from SiH 4 and NH 3 [4,5]. For comparison with the backscattering data in this work, other structure dependent measurements as etching rate and index of refraction have been performed.…”
Abstract-Backscattering and channeling effect measurements of I MeV 4He+ ions were used to determine the composition and density of SixNy layers on single crystal silicon. The nitride layers were deposited by the reaction between SiH 4 and N 2 in a glow discharge at 350°C. The ratio N/Si in the layer decreases with increasing SiH 4 concentration and total pressure of the reaction gases whereas the density is nearly constant. Conditions for deposition of stoichiometric nitride layers were optimized. These results are in good agreement with measurements of etching rate and index of refraction. Thecomposition of all sampies is homogeneous over the entire layer, the silicon substrate the yield ofbackscattered particles is reduced (channeling effect) and a more accurate determination of the nitrogen concentration can be made. These techniques have been used to analyse silicon dioxide layers [3] and nitride layers from SiH 4 and NH 3 [4,5]. For comparison with the backscattering data in this work, other structure dependent measurements as etching rate and index of refraction have been performed.
“…These techniques have been used to analyse silicon dioxide layers [3] and nitride layers from SiH 4 and NH 3 [4,5]. For comparison with the backscattering data in this work, other structure dependent measurements as etching rate and index of refraction have been performed.…”
Abstract-Backscattering and channeling effect measurements of I MeV 4He+ ions were used to determine the composition and density of SixNy layers on single crystal silicon. The nitride layers were deposited by the reaction between SiH 4 and N 2 in a glow discharge at 350°C. The ratio N/Si in the layer decreases with increasing SiH 4 concentration and total pressure of the reaction gases whereas the density is nearly constant. Conditions for deposition of stoichiometric nitride layers were optimized. These results are in good agreement with measurements of etching rate and index of refraction. Thecomposition of all sampies is homogeneous over the entire layer, the silicon substrate the yield ofbackscattered particles is reduced (channeling effect) and a more accurate determination of the nitrogen concentration can be made. These techniques have been used to analyse silicon dioxide layers [3] and nitride layers from SiH 4 and NH 3 [4,5]. For comparison with the backscattering data in this work, other structure dependent measurements as etching rate and index of refraction have been performed.
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