2004
DOI: 10.1016/j.inoche.2004.02.003
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A novel route for the preparation of monodisperse silver nanoparticles via a pulsed sonoelectrochemical technique

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Cited by 97 publications
(44 citation statements)
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“…In terms of pulsed ultrasound that is often used to prepare silver NPs [70], surfactant or organic capping reagents are often needed in the shape-selective synthesis of NPs, because they control the growth of crystals by selectively adhering to certain crystallographic planes. When introducing ultrasound to electrochemistry, mono-disperse dendritic nanostructure can be synthesised.…”
Section: Ag Dendrites Fabrication Via Electrochemical Methodsmentioning
confidence: 99%
See 1 more Smart Citation
“…In terms of pulsed ultrasound that is often used to prepare silver NPs [70], surfactant or organic capping reagents are often needed in the shape-selective synthesis of NPs, because they control the growth of crystals by selectively adhering to certain crystallographic planes. When introducing ultrasound to electrochemistry, mono-disperse dendritic nanostructure can be synthesised.…”
Section: Ag Dendrites Fabrication Via Electrochemical Methodsmentioning
confidence: 99%
“…PVP also affects the morphology of Ag NPs with different electrolyte solution. When using a saturated solution of silver citrate, the prepared silver NPs can only agglomerated to be dendritic crystals without PVP owing to the dissociation equilibrium of Ag 3 C 6 H 5 O 7 [70]. While in AgClO 4 solution, it is worth to mention that PVP favours the formation of side branches and leaves and promotes the formation of finer and more hierarchical nanostructures [72].…”
Section: Ag Dendrites Fabrication Via Electrochemical Methodsmentioning
confidence: 99%
“…Aqueous dispersions of Ag and Cu NPs can also be obtained by electrolysis of a metal salt in solution [84][85][86][87][88] and by sonochemical [89][90][91], and sonoelectrochemical [92][93][94][95] methods.…”
Section: Preparation Of Metal Npsmentioning
confidence: 99%
“…The most frequently used is poly(N-vinyl-2-pyrrolidone) (PVP) of various molecular weights, which exhibits a highly effective protective function in both organic and aqueous media. PVP has been shown to be an effective stabilizer of aqueous dispersions of Ag and Cu NPs [67,79,[93][94][95][100][101][102][103][104][105][106][107][108] as well as an effective stabilizer of Ag and Cu NPs in organic solvents [69,101,109] and especially in polyol synthesis [61,77,78,110]. The polyol method, while using PVP as a stabilizer, was utilized in the preparation of Ag and Cu NPs (size range of 40-50 nm) as precursors of metal-based conductive inks [111][112][113][114][115].…”
Section: Stabilization Of Metal Nps Against Aggregationmentioning
confidence: 99%
“…In particular, its interlayer space has been used for the synthesis of material and biomaterial NPs as the support for anchoring transition metal complex catalysts and as adsorbents for cationic ions. 30,31 In addition, various production methods have been described for the synthesis of Ag-NP colloids using silver salt as the initial materials; for instance, chemical reduction, [32][33][34][35] aerosol spraying technique, 36 reverse micelle, 37 lamellar liquid crystal, 38 microemulsion, 39 micelle, 40 capping agent method, 41 and photochemical reduction (ie, microwave, 42 electron beam, 43 ultraviolet (UV)-irradiation, 44,45 and γ-irradiation). [46][47][48] Of these techniques, the use of γ-irradiation in the preparation of Ag-NPs has been demonstrated to have a number of highly advantageous properties compared with conventional chemical and photochemical methods, namely:…”
Section: Introductionmentioning
confidence: 99%