Abstract:The analysis of metals bound to proteins requires careful sample preparation. Experimental procedures involved in this area should be developed aiming to retain the metal species bound to the protein structure. Some pre-fractionation steps are commonly used and in many cases it is necessary to disrupt the lipid-protein interaction by performing lipid removal before protein extraction. This paper presents a systematic investigation on the influence of using hexane, chloroform and methanol neat or in sequence to… Show more
“…According to the FDA [14], a daily intake of 2 mg for adults is recommended. Marthe et al [26] quantified Cu in gold linseed and obtained concentrations of 19.8 to 24.2 mg kg −1 , higher than those obtained in our study (of 16.4 mg kg −1 ). The calculated LOQ for Mo was 17 ng kg −1 .…”
Section: Determination Of Cu Mo Cr As CD and Pb And Flour Samplecontrasting
“…According to the FDA [14], a daily intake of 2 mg for adults is recommended. Marthe et al [26] quantified Cu in gold linseed and obtained concentrations of 19.8 to 24.2 mg kg −1 , higher than those obtained in our study (of 16.4 mg kg −1 ). The calculated LOQ for Mo was 17 ng kg −1 .…”
Section: Determination Of Cu Mo Cr As CD and Pb And Flour Samplecontrasting
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