NiZn-ferrite thin films were deposited onto silicon and glass substrates by radio frequency magnetron sputtering at room temperature. The effects of the relative oxygen flow ratio on the structure and magnetic properties of the thin films were investigated. The study results reveal that the films deposited under higher relative oxygen flow ratio show a better crystallinity. Static magnetic measurement results indicated that the saturation magnetization of the films was greatly affected by the crystallinity, grain dimension, and cation distribution in the NiZn-ferrite films. The NiZn-ferrite thin films with a maximum saturation magnetization of 151 emucm-3, which is about 40% of the bulk NiZn ferrite, was obtained under relative oxygen flow ratio of 60%.
The ZnO and ZnO:Ce thin films were prepared by DC reactive magnetron sputtering. The structure, surface morphology, optical and photoluminescence properties of ZnO:Ce thin films were investigated. The XRD results indicated that all the samples exhibited a hexagonal wurtzite structure. The surface morphology of the films was sensitive to the Ce concentration. All the films had a higher average transmittance (more than 85%) in the visible region and a strong absorption near the band-edge of ZnO. The photoluminescence properties of the Ce-doped ZnO thin films were also studied. Blue emissions were observed from the ZnO:Ce thin films. Our results indicated that the photoluminescence properties of ZnO thin films doped with low Ce concentration were related to the intrinsic transition of Ce3+ ions. However, when the Ce concentration increased, Zni also played an important role.
A non-aqueous synthetic route has been developed for the preparation of uniform Cu nanowires with length up to tens of micrometers. Unlike commonly used one-pot synthesis approach that usually involve a fast reduction of metal precursors in the presence of reducing agents, a continuous-injection approach has been to utilized to control the speed of reaction and the concentration of Cu nuclei. In this approach, copper (II) chloride dihydrate and nickel (II) acetylacetone which are dissolved in oleylamine solutions have been injected into octadecene by a syringe-pump. The as-prepared samples have been characterized by transmission electron microscopy, scanning electron microscopy and energy-dispersive X-ray spectroscopy. The results show that the products are pure Cu nanowires which have preferred <110> growth directions. The formation mechanism and major influencing factors on the synthesis of Cu nanowires have been discussed.
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