In the treatment of methyl orange simulation printing and dyeing wastewater by catalytic wet air oxidation method, the Ru series catalysts were prepared with the equal amount impregnation method. The catalyst activity and stability were characterized by the decolorization rate of the water samples, and the eluted metal ion concentration from the catalyst of the water samples. XRD, SEM, FT-IR were used to characterize the catalysts. The results showed that: when active allocation ratio of the catalyst was Ru:Cu:Fe:Ce:La = 1:0.5:0.5:0.5:0.5, the degradation rate of methyl orange could reach up to 98.5%. And the concentration of each metal component eluted lower after the reaction, while its activity and stability were relatively high.The active component of 1wt% Ru catalyst mainly existed as the form of γ-Al2O3, RuO2, La2O3, La2CuO4 and CeO2. The surface of catalyst was relatively flat and flaky. The Ru catalyst appeared strong infrared absorption in the vicinity of 1070 cm-1, 1650 cm-1 and 3450 cm-1.
The papermaking black liquor of one Paper Mill in ChaoZhou, GuangDong Province was treated with the wet oxidation method and the influence on treatment effect with the reaction pressure was researched. Experimental results showed that the papermaking black liquor was treated by the wet oxidation method; the treatment effect was showed upward trend with the increase of the reaction pressure, and the reaction pressure of 3.5 MPa is appropriate. The papermaking black liquor was treated by the wet oxidation method, the influent pH about 8.00 showing weakly alkaline basically. The decolorization removal and turbidity removal first increases and then slightly decreases basically with the increase of reaction time.When the reaction time is 60 min, the treatment effect is overall best. The decolorization removal can reach 61.1 % and the turbidity removal can reach 73.8 %.
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