FTIR spectroscopy has been in use broadly to study microscopic areas in polymers for the last years. The FTIR transmission spectra of coumarin laser dye, polystyrene and coumarin doped polystyrene films with different doping ratio of coumarin solution have been studied. These spectra measured and explained for all films before and after Alpha irradiation with different irradiation times. All samples prepared by casting method. FTIR corroborate chemical bonds of coumarin dye molecules and polystyrene films by producing an IR absorption spectrum when increasing doping ratio of coumarin solution and when irradiation by Alpha source. There are some bonds disappeared after irradiation.

The optical properties of polyvinyl alcohol (PVA) doped TiO2 and ZnO nanoparticles respectively, were studied. PVA/TiO2 and PVA/ZnO nanoparticles were prepared by the pulsed laser ablation technique (PLA).The optical properties of PVA/ TiO2 and PVA/ ZnO nanocomposite solution have been investigated by transmittance data and absorption spectra. The optical band gap (Eg) was determined and the optical absorption spectra showed that a direct transition. The energy gap of PVA/ ZnO nanoparticles have been observed the decreases its value and increasing in the optical conductivity as compared to PVA/ TiO2.The refractive index (n), extinction coefficient (k) and dielectric constant have been also investigated; it was found that all the above parameters affects by doping.

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